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A three-stage chemical cleaning of ion-exchange membranes used in the treatment by electrodialysis of wastewaters generated in brass electroplating industries

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A three-stage chemical cleaning of ion-exchange membranes used in the treatment by electrodialysis of wastewaters generated in brass electroplating industries

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dc.contributor.author Santana Barros, Kayo es_ES
dc.contributor.author Martí Calatayud, Manuel César es_ES
dc.contributor.author Pérez-Herranz, Valentín es_ES
dc.contributor.author Espinosa, Denise Crocce Romano es_ES
dc.date.accessioned 2021-05-13T03:32:32Z
dc.date.available 2021-05-13T03:32:32Z
dc.date.issued 2020-10-15 es_ES
dc.identifier.issn 0011-9164 es_ES
dc.identifier.uri http://hdl.handle.net/10251/166271
dc.description.abstract [EN] After long-term electrodialysis, cleaning the membranes is crucial to extend their lifetime. In this work, we evaluate the effects of a three-stage chemical cleaning on electrochemical and structural properties of anion- and cation-exchange membranes. Membranes used in the electrodialytic treatment of a synthetic effluent from the cyanide-free brass electrodeposition were cleaned using 0.1, 0.5 and 1.0 mol.L-1 NaOH solutions. The electrochemical behavior of the membranes was evaluated after each cleaning step by chronopotentiometry. Additionally, changes in the membrane structure and composition were analyzed by FTIR-ATR and SEM/EDS. While the membranes undergo a decline in some electrochemical features after the electrodialysis process, the cleaning with 0.1 mol.L-1 NaOH showed to be the most effective in recovering the properties characteristic of the virgin membranes: the limiting current density increased by 84% after the cleaning, whereas the ohmic and overlimiting resistances decreased by 47% and 55%, respectively. In contrast, the 0.5 and 1.0 mol.L-1 NaOH solutions degraded the membranes and reduced their fraction of conducive area, especially for the anion-exchange one. This favored fouling/scaling occurrence, as noticed by a prominent increase in the potential drop of the anion-exchange membrane. FTIR-ATR and SEM/EDS analyses confirmed fouling/scaling, as well as degradation of the ion-exchange membranes. es_ES
dc.description.sponsorship The authors gratefully acknowledge the financial support given by funding agencies CNPq (Process 141346/2016-7) and CAPES (Process 88881.190502/2018-01). This study was financed in part by the Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior -Brasil (CAPES) -Finance Code 001. es_ES
dc.language Inglés es_ES
dc.publisher Elsevier es_ES
dc.relation.ispartof Desalination es_ES
dc.rights Reconocimiento - No comercial - Sin obra derivada (by-nc-nd) es_ES
dc.subject Alkaline cleaning es_ES
dc.subject Chronopotentiometry es_ES
dc.subject Ion-exchange membranes es_ES
dc.subject Membrane cleaning es_ES
dc.subject Membrane fouling es_ES
dc.subject.classification INGENIERIA QUIMICA es_ES
dc.title A three-stage chemical cleaning of ion-exchange membranes used in the treatment by electrodialysis of wastewaters generated in brass electroplating industries es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1016/j.desal.2020.114628 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/CAPES//001/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/CNPq//141346%2F2016-7/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/CAPES//88881.190502%2F2018-01/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Ingeniería Química y Nuclear - Departament d'Enginyeria Química i Nuclear es_ES
dc.description.bibliographicCitation Santana Barros, K.; Martí Calatayud, MC.; Pérez-Herranz, V.; Espinosa, DCR. (2020). A three-stage chemical cleaning of ion-exchange membranes used in the treatment by electrodialysis of wastewaters generated in brass electroplating industries. Desalination. 492:1-11. https://doi.org/10.1016/j.desal.2020.114628 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.1016/j.desal.2020.114628 es_ES
dc.description.upvformatpinicio 1 es_ES
dc.description.upvformatpfin 11 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 492 es_ES
dc.relation.pasarela S\416992 es_ES
dc.contributor.funder Coordenaçao de Aperfeiçoamento de Pessoal de Nível Superior, Brasil es_ES
dc.contributor.funder Conselho Nacional de Desenvolvimento Científico e Tecnológico, Brasil es_ES
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