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Multiple-scan voltammetry of immobilized particles of ancient copper/bronze coins

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Multiple-scan voltammetry of immobilized particles of ancient copper/bronze coins

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dc.contributor.author Domenech Carbo, Antonio es_ES
dc.contributor.author Donnici, Margherita es_ES
dc.contributor.author Álvarez-Romero, Carla es_ES
dc.contributor.author Daniele, Salvatore es_ES
dc.contributor.author Domenech Carbo, Mª Teresa es_ES
dc.date.accessioned 2022-10-18T18:03:32Z
dc.date.available 2022-10-18T18:03:32Z
dc.date.issued 2021-01 es_ES
dc.identifier.issn 1432-8488 es_ES
dc.identifier.uri http://hdl.handle.net/10251/188193
dc.description.abstract [EN] The application of a multiple-scan strategy to study the structure of the corrosion patina of copper/bronze ancient objects using the voltammetry of immobilized microparticles (VIMP) is described. Upon nanosample attachment to graphite electrodes in contact with aqueous acetate buffer, voltammetric signatures characterizing cuprite with variable degree of crystallinity are recorded by means of successive cathodic scans reflecting the composition of the corrosion patina. The reported methodology, complemented with ion beam-field emission scanning electron microscopy (FIB-FESEM) and high-resolution field emission scanning electron microscopy (HRFESM-EDX), is applied to a set of coins fabricated between 1709 and 1962 revealing different corrosion patterns. es_ES
dc.description.sponsorship Project CTQ2017-85317-C2-1-P, supported with Ministerio de Economia, Industria y Competitividad (MINECO), Fondo Europeo de Desarrollo Regional (ERDF) and Agencia Estatal de Investigacion (AEI), is gratefully acknowledged. The authors wish to thank Mr. Manuel Planes, Dr. Jose Luis Moya and Alicia Nuez Imbernon technical supervisors of the Electron Microscopy Service of the Polytechnical University of Valencia. es_ES
dc.language Inglés es_ES
dc.publisher Springer-Verlag es_ES
dc.relation.ispartof Journal of Solid State Electrochemistry es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Voltammetry of immobilized particles es_ES
dc.subject Copper es_ES
dc.subject Bronze es_ES
dc.subject Corrosion es_ES
dc.subject.classification PINTURA es_ES
dc.title Multiple-scan voltammetry of immobilized particles of ancient copper/bronze coins es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1007/s10008-020-04770-4 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/CTQ2017-85317-C2-1-P/ES/APLICACION DE TECNICAS AVANZADAS DE MICROSCOPIA EN EL ESTUDIO DEL PATRIMONIO CERAMICO Y VITREO/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/PID2020-113022GB-I00/ES/APLICACION DE TECNICAS AVANZADAS DE ELECTROQUIMICA DE ESTADO SOLIDO Y MICROSCOPIA EN EL ESTUDIO DE RESTOS ARQUEOLOGICOS DE NATURALEZA ORGANICA/ es_ES
dc.rights.accessRights Cerrado es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Conservación y Restauración de Bienes Culturales - Departament de Conservació i Restauració de Béns Culturals es_ES
dc.description.bibliographicCitation Domenech Carbo, A.; Donnici, M.; Álvarez-Romero, C.; Daniele, S.; Domenech Carbo, MT. (2021). Multiple-scan voltammetry of immobilized particles of ancient copper/bronze coins. Journal of Solid State Electrochemistry. 25(1):195-206. https://doi.org/10.1007/s10008-020-04770-4 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.1007/s10008-020-04770-4 es_ES
dc.description.upvformatpinicio 195 es_ES
dc.description.upvformatpfin 206 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 25 es_ES
dc.description.issue 1 es_ES
dc.relation.pasarela S\459606 es_ES
dc.contributor.funder AGENCIA ESTATAL DE INVESTIGACION es_ES
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