- -

Dating archaeological copper using electrochemical impedance spectroscopy. Comparison with voltammetry of microparticles dating

RiuNet: Repositorio Institucional de la Universidad Politécnica de Valencia

Compartir/Enviar a

Citas

Estadísticas

  • Estadisticas de Uso

Dating archaeological copper using electrochemical impedance spectroscopy. Comparison with voltammetry of microparticles dating

Mostrar el registro sencillo del ítem

Ficheros en el ítem

Thumbnail
Nombre: ArticleCuDatingMa ...
Tamaño: 615.3Kb
Formato: PDF
Descripción: Versión del Autor.
Abrir
[Cerrado]
Nombre: MaterCorrosCu.pdf
Tamaño: 708.6Kb
Formato: PDF
Descripción: Versión editorial
Solicitar una copia al autor
dc.contributor.author Domenech Carbo, Antonio es_ES
dc.contributor.author Capelo, Sofia es_ES
dc.contributor.author Piquero-Cilla, Juan es_ES
dc.contributor.author Domenech Carbo, Mª Teresa es_ES
dc.contributor.author Barrio, J. es_ES
dc.contributor.author Fuentes, A. es_ES
dc.contributor.author Al sekhaneh, W. es_ES
dc.date.accessioned 2018-07-06T07:21:03Z
dc.date.available 2018-07-06T07:21:03Z
dc.date.issued 2016 es_ES
dc.identifier.issn 0947-5117 es_ES
dc.identifier.uri http://hdl.handle.net/10251/105410
dc.description.abstract [EN] A methodology for dating copper/bronze archaeological objects aged under atmospheric environments using electrochemical impedance spectroscopy (EIS) is described. The method is based on the measurement of resistance associated to the growth of corrosion layers in EIS recorded upon immersion of the pieces in mineral water and applying a bias potential for the reduction of dissolved oxygen. Theoretical expressions for the time variation of such resistance following a potential rate law are presented. Equivalent expressions are derived and applied for estimating the variation of the tenorite/cuprite ratio from their specific voltammetric signals using voltammetry of microparticles data. Calibration curves were constructed from a set of well-documented coins. es_ES
dc.description.sponsorship Financial support from the MEC Projects CTQ2011-28079-CO3-01 and 02 and CTQ2014-53736-C3-2-P which are supported with ERDF funds is gratefully acknowledged. es_ES
dc.language Inglés es_ES
dc.publisher John Wiley & Sons es_ES
dc.relation.ispartof Materials and Corrosion es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Archaeological copper es_ES
dc.subject Electrochemical Impedance Spectroscopy es_ES
dc.subject Voltammetry of microparticles es_ES
dc.subject Dating es_ES
dc.subject Conservation-restoration es_ES
dc.subject.classification PINTURA es_ES
dc.title Dating archaeological copper using electrochemical impedance spectroscopy. Comparison with voltammetry of microparticles dating es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1002/maco.201408048 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MICINN//CTQ2011-28079-C03-01/ES/DESARROLLO DE METODOS NANOELECTROQUIMICOS DE ANALISIS DE OBRA PICTORICA BASADOS EN LA TECNICA DE MICROSCOPIA DE FUERZA ATOMICA-VOLTAMETRIA DE NANOPARTICULAS/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//CTQ2014-53736-C3-1-P/ES/APLICACION DE LAS TECNICAS NANOELECTROQUIMICAS Y BIOTECNOLOGIAS EN EL ESTUDIO Y CONSERVACION DEL PATRIMONIO EN METAL/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Conservación y Restauración de Bienes Culturales - Departament de Conservació i Restauració de Béns Culturals es_ES
dc.description.bibliographicCitation Domenech Carbo, A.; Capelo, S.; Piquero-Cilla, J.; Domenech Carbo, MT.; Barrio, J.; Fuentes, A.; Al Sekhaneh, W. (2016). Dating archaeological copper using electrochemical impedance spectroscopy. Comparison with voltammetry of microparticles dating. Materials and Corrosion. 67(2):120-129. https://doi.org/10.1002/maco.201408048 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://doi.org/10.1002/maco.201408048 es_ES
dc.description.upvformatpinicio 120 es_ES
dc.description.upvformatpfin 129 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 67 es_ES
dc.description.issue 2 es_ES
dc.relation.pasarela S\326838 es_ES
dc.contributor.funder Ministerio de Ciencia e Innovación es_ES
dc.description.references Friedman, I., & Smith, R. L. (1960). Part I, The Development of the Method. American Antiquity, 25(4), 476-493. doi:10.2307/276634 es_ES
dc.description.references Reich, S., Leitus, G., & Shalev, S. (2003). Measurement of corrosion content of archaeological lead artifacts by their Meissner response in the superconducting state; a new dating method. New Journal of Physics, 5, 99-99. doi:10.1088/1367-2630/5/1/399 es_ES
dc.description.references Scholz, F., Schröder, U., Meyer, S., Brainina, K. Z., Zakhachuk, N. F., Sobolev, N. V., & Kozmenko, O. A. (1995). The electrochemical response of radiation defects of non-conducting materials An electrochemical access to age determinations. Journal of Electroanalytical Chemistry, 385(1), 139-142. doi:10.1016/0022-0728(94)03840-y es_ES
dc.description.references Doménech-Carbó, A., Labuda, J., & Scholz, F. (2012). Electroanalytical chemistry for the analysis of solids: Characterization and classification (IUPAC Technical Report). Pure and Applied Chemistry, 85(3), 609-631. doi:10.1351/pac-rep-11-11-13 es_ES
dc.description.references Doménech-Carbó, A., Doménech-Carbó, M. T., & Costa, V. (Eds.). (2009). Electrochemical Methods in Archaeometry, Conservation and Restoration. Monographs in Electrochemistry. doi:10.1007/978-3-540-92868-3 es_ES
dc.description.references Doménech-Carbó, A., Doménech-Carbó, M. T., & Peiró-Ronda, M. A. (2011). Dating Archeological Lead Artifacts from Measurement of the Corrosion Content Using the Voltammetry of Microparticles. Analytical Chemistry, 83(14), 5639-5644. doi:10.1021/ac200731q es_ES
dc.description.references Doménech-Carbó, A., Doménech-Carbó, M. T., Capelo, S., Pasíes, T., & Martínez-Lázaro, I. (2014). Dating Archaeological Copper/Bronze Artifacts by Using the Voltammetry of Microparticles. Angewandte Chemie International Edition, 53(35), 9262-9266. doi:10.1002/anie.201404522 es_ES
dc.description.references Benarie, M., & Lipfert, F. L. (1986). A general corrosion function in terms of atmospheric pollutant concentrations and rain pH. Atmospheric Environment (1967), 20(10), 1947-1958. doi:10.1016/0004-6981(86)90336-7 es_ES
dc.description.references Strandberg, H. (1998). Reactions of copper patina compounds—II. influence of sodium chloride in the presence of some air pollutants. Atmospheric Environment, 32(20), 3521-3526. doi:10.1016/s1352-2310(98)00058-2 es_ES
dc.description.references Cano, E., Lafuente, D., & Bastidas, D. M. (2009). Use of EIS for the evaluation of the protective properties of coatings for metallic cultural heritage: a review. Journal of Solid State Electrochemistry, 14(3), 381-391. doi:10.1007/s10008-009-0902-6 es_ES
dc.description.references Hernandez-Escampa, M., Gonzalez, J., & Uruchurtu-Chavarin, J. (2009). Electrochemical assessment of the restoration and conservation of a heavily corroded archaeological iron artifact. Journal of Applied Electrochemistry, 40(2), 345-356. doi:10.1007/s10800-009-0003-3 es_ES
dc.description.references Angelini, E., Grassini, S., Parvis, M., & Zucchi, F. (2011). An in situ investigation of the corrosion behaviour of a weathering steel work of art. Surface and Interface Analysis, 44(8), 942-946. doi:10.1002/sia.3842 es_ES
dc.description.references Grassini, S., Angelini, E., Parvis, M., Bouchar, M., Dillmann, P., & Neff, D. (2013). An in situ corrosion study of Middle Ages wrought iron bar chains in the Amiens Cathedral. Applied Physics A, 113(4), 971-979. doi:10.1007/s00339-013-7724-1 es_ES
dc.description.references Doménech-Carbó, A., Doménech-Carbó, M. T., Peiró-Ronda, M. A., Martínez-Lázaro, I., & Barrio-Martín, J. (2012). Application of the voltammetry of microparticles for dating archaeological lead using polarization curves and electrochemical impedance spectroscopy. Journal of Solid State Electrochemistry, 16(7), 2349-2356. doi:10.1007/s10008-012-1668-9 es_ES
dc.description.references Degrigny, C., Guibert, G., Ramseyer, S., Rapp, G., & Tarchini, A. (2009). Use of E corr vs time plots for the qualitative analysis of metallic elements from scientific and technical objects: the SPAMT Test Project. Journal of Solid State Electrochemistry, 14(3), 425-435. doi:10.1007/s10008-009-0890-6 es_ES
dc.description.references Souissi, N., Bousselmi, L., Khosrof, S., & Triki, E. (2004). Voltammetric behaviour of an archeaological bronze alloy in aqueous chloride media. Materials and Corrosion, 55(4), 284-292. doi:10.1002/maco.200303719 es_ES
dc.description.references Souissi, N., Triki, E., Bousselmi, L., & Khosrof, S. (2006). Comparaison between archaeological and artificially aged bronze interfaces. Materials and Corrosion, 57(10), 794-799. doi:10.1002/maco.200503974 es_ES
dc.description.references Souissi, N., & Triki, E. (2009). Characterization of ethnographic copper corrosion. Materials and Corrosion, 60(4), 262-268. doi:10.1002/maco.200805068 es_ES
dc.description.references Mata, A. L., Salta, M. M. L., Neto, M. M. M., Mendonça, M. H., & Fonseca, I. T. E. (2010). Characterization of two Roman coins from an archaeological site in Portugal. Materials and Corrosion, 61(3), 205-210. doi:10.1002/maco.200905284 es_ES
dc.description.references Feliu, S., Morcillo, M., & Feliu, S. (1993). The prediction of atmospheric corrosion from meteorological and pollution parameters—II. Long-term forecasts. Corrosion Science, 34(3), 415-422. doi:10.1016/0010-938x(93)90113-u es_ES
dc.description.references Spence, J. W., Haynie, F. H., Lipfert, F. W., Cramer, S. D., & McDonald, L. G. (1992). Atmospheric Corrosion Model for Galvanized Steel Structures. CORROSION, 48(12), 1009-1019. doi:10.5006/1.3315903 es_ES
dc.description.references Bhattacharjee, S., Roy, N., Dey, A. K., & Banerjee, M. K. (1993). Statistical appraisal of the atmospheric corrosion of mild steel. Corrosion Science, 34(4), 573-581. doi:10.1016/0010-938x(93)90273-j es_ES
dc.description.references Kobus, J. (2000). Long-term atmospheric corrosion monitoring. Materials and Corrosion, 51(2), 104-108. doi:10.1002/(sici)1521-4176(200002)51:2<104::aid-maco104>3.0.co;2-v es_ES
dc.description.references Balasubramaniam, R., Laha, T., & Srivastava, A. (2004). Long term corrosion behaviour of copper in soil: A study of archaeological analogues. Materials and Corrosion, 55(3), 194-202. doi:10.1002/maco.200303723 es_ES
dc.description.references Natesan, M., Venkatachari, G., & Palaniswamy, N. (2006). Kinetics of atmospheric corrosion of mild steel, zinc, galvanized iron and aluminium at 10 exposure stations in India. Corrosion Science, 48(11), 3584-3608. doi:10.1016/j.corsci.2006.02.006 es_ES
dc.description.references Doménech, A., Doménech-Carbó, M. T., Pasies, T., & del Carmen Bouzas, M. (2012). Modeling Corrosion of Archaeological Silver-Copper Coins Using the Voltammetry of Immobilized Particles. Electroanalysis, 24(10), 1945-1955. doi:10.1002/elan.201200252 es_ES
dc.description.references Rosas-Camacho, O., Uquidi-Macdonald, M., & Macdonald, D. D. (2009). Deterministic Modeling of the Corrosion of Low-Carbon Steel by Dissolved Carbon Dioxide and the Effect of Acetic Acid. I-Effect of Carbon Dioxide. doi:10.1149/1.3259806 es_ES
dc.description.references Macdonald, D., & Englehardt, G. (2010). The Point Defect Model for Bi-Layer Passive Films. doi:10.1149/1.3496427 es_ES
dc.description.references Sharifi-Asl, S., Taylor, M. L., Lu, Z., Engelhardt, G. R., Kursten, B., & Macdonald, D. D. (2013). Modeling of the electrochemical impedance spectroscopic behavior of passive iron using a genetic algorithm approach. Electrochimica Acta, 102, 161-173. doi:10.1016/j.electacta.2013.03.143 es_ES
dc.description.references Macdonald, D. D. (2011). The history of the Point Defect Model for the passive state: A brief review of film growth aspects. Electrochimica Acta, 56(4), 1761-1772. doi:10.1016/j.electacta.2010.11.005 es_ES
dc.description.references Doménech-Carbó, A., Lastras, M., Rodríguez, F., Cano, E., Piquero-Cilla, J., & Osete-Cortina, L. (2013). Monitoring stabilizing procedures of archaeological iron using electrochemical impedance spectroscopy. Journal of Solid State Electrochemistry, 18(2), 399-409. doi:10.1007/s10008-013-2232-y es_ES
dc.description.references Blum, D., Leyffer, W., & Holze, R. (1996). Pencil-Leads as new electrodes for abrasive stripping voltammetry. Electroanalysis, 8(3), 296-297. doi:10.1002/elan.1140080317 es_ES
dc.description.references Doménech-Carbó, A., Doménech-Carbó, M. T., & Peiró-Ronda, Mªa. (2011). ‘One-Touch’ Voltammetry of Microparticles for the Identification of Corrosion Products in Archaeological Lead. Electroanalysis, 23(6), 1391-1400. doi:10.1002/elan.201000739 es_ES
dc.description.references Nair, M. T. ., Guerrero, L., Arenas, O. L., & Nair, P. . (1999). Chemically deposited copper oxide thin films: structural, optical and electrical characteristics. Applied Surface Science, 150(1-4), 143-151. doi:10.1016/s0169-4332(99)00239-1 es_ES
dc.description.references Scott, D. A. (1997). Copper compounds in metals and colorants: oxides and hydroxides. Studies in Conservation, 42(2), 93-100. doi:10.1179/sic.1997.42.2.93 es_ES
dc.description.references Doménech, A., Doménech-Carbó, M. T., & Martínez-Lázaro, I. (2010). Layer-by-layer identification of copper alteration products in metallic works of art using the voltammetry of microparticles. Analytica Chimica Acta, 680(1-2), 1-9. doi:10.1016/j.aca.2010.09.002 es_ES
dc.description.references Doménech, A., Doménech-Carbó, M. T., Pasies, T., & Bouzas, M. C. (2011). Application of Modified Tafel Analysis to the Identification of Corrosion Products on Archaeological Metals Using Voltammetry of Microparticles. Electroanalysis, 23(12), 2803-2812. doi:10.1002/elan.201100577 es_ES
dc.description.references Li, W. S., Cai, S. Q., & Luo, J. L. (2004). Chronopotentiometric Responses and Capacitance Behaviors of Passive Film Formed on Iron in Borate Buffer Solution. Journal of The Electrochemical Society, 151(4), B220. doi:10.1149/1.1667521 es_ES
dc.description.references Liu, W., Zhang, H., Qu, Z., Zhang, Y., & Li, J. (2009). Corrosion behavior of the steel used as a huge storage tank in seawater. Journal of Solid State Electrochemistry, 14(6), 965-973. doi:10.1007/s10008-009-0886-2 es_ES
dc.description.references Toledo-Matos, L. A., & Pech-Canul, M. A. (2010). Evolution of an iron passive film in a borate buffer solution (pH 8.4). Journal of Solid State Electrochemistry, 15(9), 1927-1934. doi:10.1007/s10008-010-1213-7 es_ES
dc.description.references Park, J.-J., & Pyun, S.-I. (2003). Analysis of impedance spectra of a pitted Inconel alloy 600 electrode in chloride ion-containing thiosulfate solution at temperatures of 298–573 K. Journal of Solid State Electrochemistry, 7(6), 380-388. doi:10.1007/s10008-002-0346-8 es_ES
dc.description.references Ibrahim, M. A., Pongkao, D., & Yoshimura, M. (2001). The electrochemical behavior and characterization of the anodic oxide film formed on titanium in NaOH solutions. Journal of Solid State Electrochemistry, 6(5), 341-350. doi:10.1007/s100080100229 es_ES
dc.description.references Xia, Z., Nanjo, H., Aizawa, T., Kanakubo, M., Fujimura, M., & Onagawa, J. (2007). Growth process of atomically flat anodic films on titanium under potentiostatical electrochemical treatment in H2SO4 solution. Surface Science, 601(22), 5133-5141. doi:10.1016/j.susc.2007.04.211 es_ES
dc.description.references Acevedo-Peña, P., Vázquez, G., Laverde, D., Pedraza-Rosas, J. E., & González, I. (2009). Influence of structural transformations over the electrochemical behavior of Ti anodic films grown in 0.1 M NaOH. Journal of Solid State Electrochemistry, 14(5), 757-767. doi:10.1007/s10008-009-0838-x es_ES
dc.description.references Fabregat-Santiago, F., Bisquert, J., Garcia-Belmonte, G., Boschloo, G., & Hagfeldt, A. (2005). Influence of electrolyte in transport and recombination in dye-sensitized solar cells studied by impedance spectroscopy. Solar Energy Materials and Solar Cells, 87(1-4), 117-131. doi:10.1016/j.solmat.2004.07.017 es_ES
dc.description.references Rubinstein, I. (1987). Electrochemical Impedance Analysis of Polyaniline Films on Electrodes. Journal of The Electrochemical Society, 134(12), 3078. doi:10.1149/1.2100343 es_ES
dc.description.references Lee, S.-J., & Pyun, S.-I. (2006). Assessment of corrosion resistance of surface-coated galvanized steel by analysis of the AC impedance spectra measured on the salt-spray-tested specimen. Journal of Solid State Electrochemistry, 11(6), 829-839. doi:10.1007/s10008-006-0229-5 es_ES
dc.description.references Doménech, A., Doménech-Carbó, M. T., & Edwards, H. G. M. (2008). Quantitation from Tafel Analysis in Solid-State Voltammetry. Application to the Study of Cobalt and Copper Pigments in Severely Damaged Frescoes. Analytical Chemistry, 80(8), 2704-2716. doi:10.1021/ac7024333 es_ES
dc.description.references Mora, N., Cano, E., Polo, J. L., Puente, J. M., & Bastidas, J. M. (2004). Corrosion protection properties of cerium layers formed on tinplate. Corrosion Science, 46(3), 563-578. doi:10.1016/s0010-938x(03)00171-9 es_ES
dc.description.references Bastidas, J. M., Polo, J. L., Cano, E., Torres, C. L., & Mora, N. (2000). Localised corrosion of highly alloyed stainless steels in an ammonium chloride and diethylamine chloride aqueous solution. Materials and Corrosion, 51(10), 712-718. doi:10.1002/1521-4176(200010)51:10<712::aid-maco712>3.0.co;2-v es_ES
dc.description.references Xu, J., Huang, W., & McCreery, R. L. (1996). Isotope and surface preparation effects on alkaline dioxygen reduction at carbon electrodes. Journal of Electroanalytical Chemistry, 410(2), 235-242. doi:10.1016/0022-0728(96)04545-7 es_ES
dc.description.references Kuang, F., Zhang, D., Li, Y., Wan, Y., & Hou, B. (2008). Electrochemical impedance spectroscopy analysis for oxygen reduction reaction in 3.5% NaCl solution. Journal of Solid State Electrochemistry, 13(3), 385-390. doi:10.1007/s10008-008-0570-y es_ES
dc.description.references Chen, G., Waraksa, C. C., Cho, H., Macdonald, D. D., & Mallouka, T. E. (2003). EIS Studies of Porous Oxygen Electrodes with Discrete Particles. Journal of The Electrochemical Society, 150(9), E423. doi:10.1149/1.1594729 es_ES


Este ítem aparece en la(s) siguiente(s) colección(ones)

Mostrar el registro sencillo del ítem