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Electrochemical analysis of gold embroidery threads from archeological textiles

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Electrochemical analysis of gold embroidery threads from archeological textiles

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dc.contributor.author Martínez, Betlem es_ES
dc.contributor.author Piquero-Cilla, Juan es_ES
dc.contributor.author Domenech Carbo, Mª Teresa es_ES
dc.contributor.author Montoya, Noemí es_ES
dc.contributor.author DOMÉNECH CARBÓ, ANTONIO es_ES
dc.date.accessioned 2019-07-31T20:02:16Z
dc.date.available 2019-07-31T20:02:16Z
dc.date.issued 2018 es_ES
dc.identifier.issn 1432-8488 es_ES
dc.identifier.uri http://hdl.handle.net/10251/124601
dc.description.abstract [EN] A methodology for characterizing archeological gold embroidery threads based on two analytical techniques is described: Field emission scanning electron microscopy (FESEM-EDX) and voltammetry of immobilized microparticle (VIMP) methodologies. After the analysis of the chemical composition of the metallic foil, we analyze specific voltammetric features associated with the oxidation of gold in contact with aqueous H2SO4 and HCl electrolytes. Cyclic and square wave voltammetries (VMP) have been used to get information about the elemental composition and the corrosion products of the samples. AFM, FESEM-EDX, and FESEM-FIB-EDX methodologies complete the study and bring us closer to the composition of the alloys and the embroidery manufacture techniques. This technique actualizes the VIMP data and evidences the morphological and elemental differences between them; in particular, it is confirmed that Au-Ag-Cu alloys, with notably differences in Ag content depending on the provenance, were used. es_ES
dc.description.sponsorship Projects CTQ2014-53736-C3-1-P and CTQ2014-53736-C3-2P, which are supported with Ministerio de Economia, Industria y Competitividad (MINECO), and Fondo Europeo de Desarrollo Regional (ERDF) funds, as well as project CTQ2017-85317-C2-1-P supported with funds from MINECO, ERDF, and Agencia Estatal de Investigacion (AEI), are gratefully acknowledged. es_ES
dc.language Inglés es_ES
dc.publisher Springer-Verlag es_ES
dc.relation.ispartof Journal of Solid State Electrochemistry es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Gilding es_ES
dc.subject Voltammetry of microparticles es_ES
dc.subject FESEM-FIB-EDX es_ES
dc.subject AFM es_ES
dc.subject Aging es_ES
dc.subject.classification PINTURA es_ES
dc.title Electrochemical analysis of gold embroidery threads from archeological textiles es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1007/s10008-018-3927-x es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//CTQ2014-53736-C3-1-P/ES/APLICACION DE LAS TECNICAS NANOELECTROQUIMICAS Y BIOTECNOLOGIAS EN EL ESTUDIO Y CONSERVACION DEL PATRIMONIO EN METAL/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/CTQ2017-85317-C2-1-P/ES/APLICACION DE TECNICAS AVANZADAS DE MICROSCOPIA EN EL ESTUDIO DEL PATRIMONIO CERAMICO Y VITREO/ es_ES
dc.rights.accessRights Abierto es_ES
dc.date.embargoEndDate 2019-07-31 es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Conservación y Restauración de Bienes Culturales - Departament de Conservació i Restauració de Béns Culturals es_ES
dc.description.bibliographicCitation Martínez, B.; Piquero-Cilla, J.; Domenech Carbo, MT.; Montoya, N.; Doménech Carbó, A. (2018). Electrochemical analysis of gold embroidery threads from archeological textiles. Journal of Solid State Electrochemistry. 22(7):2205-2215. https://doi.org/10.1007/s10008-018-3927-x es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.1007/s10008-018-3927-x es_ES
dc.description.upvformatpinicio 2205 es_ES
dc.description.upvformatpfin 2215 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 22 es_ES
dc.description.issue 7 es_ES
dc.relation.pasarela S\379550 es_ES
dc.contributor.funder Agencia Estatal de Investigación es_ES
dc.contributor.funder Ministerio de Economía y Competitividad es_ES
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