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Ultrasound and Microwave Assisted Extraction of Opuntia Fruit Peels Biocompounds: Optimization and Comparison Using RSM-CCD

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Ultrasound and Microwave Assisted Extraction of Opuntia Fruit Peels Biocompounds: Optimization and Comparison Using RSM-CCD

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dc.contributor.author Melgar-Castañeda, Bruno es_ES
dc.contributor.author Dias, Maria Inês es_ES
dc.contributor.author Barros, L. es_ES
dc.contributor.author Ferreira, I. CFR es_ES
dc.contributor.author Rodríguez López, Antonio Diego es_ES
dc.contributor.author Garcia-Castello, Esperanza M. es_ES
dc.date.accessioned 2020-05-14T03:04:55Z
dc.date.available 2020-05-14T03:04:55Z
dc.date.issued 2019-10-08 es_ES
dc.identifier.issn 1420-3049 es_ES
dc.identifier.uri http://hdl.handle.net/10251/143136
dc.description.abstract [EN] Ultrasound-assisted extraction (UAE) and microwave-assisted extraction (MAE) of bioactive compounds, peels from Opuntia engelmannii cultivar (cv.) Valencia were optimized by response surface methodology. Randomized extraction runs were performed for each of the technologies employed in order to build effective models with maximum (bioactive molecules content and yield) and minimum (antioxidant activity) responses. A 5-level, 4-factor central composite design was used to obtain target responses as a function of extraction time (t), solid to liquid ratio (S/L), methanol concentration (metOH), and temperature (T). Specific response optimization for each technology was analyzed, discussed, and general optimization from all the responses together was also gather. The optimum values for each factor were: t = 2.5 and 1.4 min, S/L = 5 and 5 g/L, metOH = 34.6 and 0% of methanol and T = 30 and 36.6 °C, achieving maximum responses of 201.6 and 132.9 mg of betalains/g, 13.9 and 8.0 mg of phenolic acids/g, 2.4 and 1.5 mg of flavonoids/g, 71.8% and 79.1% of extractable solid and IC50 values for the antioxidant activity of 2.9 and 3.6, for UAE and MAE, respectively. The present study suggested UAE as the best extraction system, in order to maximize recovery of bioactive compounds with a high antioxidant activity. es_ES
dc.description.sponsorship The authors are grateful to the Foundation for Science and Technology (FCT, Portugal) and FEDER under Programmer PT2020 for financial support to CIMO (UID/AGR/00690/2019) and L. Barros and M.I. Dias also thank the national funding by FCT, P.I., through the institutional scientific employment program-contract. The authors are grateful to CONACyT for supporting B. Melgar with his doctoral grant (No. 329930). The authors specially thanks to Maria Luisa Ruiz and the "Laboratorio Agroalimentario de la Comunitat Valenciana" for allow the use of the microwave for the extractions. This work is also funded by the European Regional Development Fund (ERDF) through the Regional Operational Program North 2020, within the scope of Project Mobilizador Norte-01-0247-FEDER-024479: ValorNatural(R) es_ES
dc.language Inglés es_ES
dc.publisher MDPI AG es_ES
dc.relation.ispartof Molecules es_ES
dc.rights Reconocimiento (by) es_ES
dc.subject Opuntia es_ES
dc.subject By-products es_ES
dc.subject Phenolic compounds es_ES
dc.subject Betalains es_ES
dc.subject Extraction optimization es_ES
dc.subject Response Surface Methodology (RSM) es_ES
dc.subject.classification INGENIERIA QUIMICA es_ES
dc.title Ultrasound and Microwave Assisted Extraction of Opuntia Fruit Peels Biocompounds: Optimization and Comparison Using RSM-CCD es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.3390/molecules24193618 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/FCT//NORTE-01-0247-FEDER-024479/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/FCT//UID%2FAGR%2F00690%2F2019/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/CONACyT//329930/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Ingeniería Química y Nuclear - Departament d'Enginyeria Química i Nuclear es_ES
dc.description.bibliographicCitation Melgar-Castañeda, B.; Dias, MI.; Barros, L.; Ferreira, IC.; Rodríguez López, AD.; Garcia-Castello, EM. (2019). Ultrasound and Microwave Assisted Extraction of Opuntia Fruit Peels Biocompounds: Optimization and Comparison Using RSM-CCD. Molecules. 24(19):1-16. https://doi.org/10.3390/molecules24193618 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.3390/molecules24193618 es_ES
dc.description.upvformatpinicio 1 es_ES
dc.description.upvformatpfin 16 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 24 es_ES
dc.description.issue 19 es_ES
dc.identifier.pmid 31597259 es_ES
dc.identifier.pmcid PMC6804160 es_ES
dc.relation.pasarela S\394931 es_ES
dc.contributor.funder European Regional Development Fund es_ES
dc.contributor.funder Consejo Nacional de Ciencia y Tecnología, México es_ES
dc.contributor.funder Fundação para a Ciência e a Tecnologia, Portugal es_ES
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