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Electrochemical analysis of the first Polish coins using voltammetry of immobilized particles

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Electrochemical analysis of the first Polish coins using voltammetry of immobilized particles

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dc.contributor.author Doménech Carbó, Antonio es_ES
dc.contributor.author Del Hoyo Meléndez, Julio M. es_ES
dc.contributor.author Domenech Carbo, Mª Teresa es_ES
dc.contributor.author Piquero-Cilla, Juan es_ES
dc.date.accessioned 2020-07-31T03:31:14Z
dc.date.available 2020-07-31T03:31:14Z
dc.date.issued 2017-01 es_ES
dc.identifier.issn 0026-265X es_ES
dc.identifier.uri http://hdl.handle.net/10251/149076
dc.description.abstract [EN] A series of 20 denarii from Boleslaus the Brave (992-1025) and Mieszko II Lambert (1025-1034), corresponding to the beginning of the Polish state were studied using the voltammetry of immobilized particles (VIMP) methodology. VIMP experiments, applied to nanosamples of the corrosion layers of the coins in contact with aqueous acetate buffer, provided well-defined responses mainly corresponding to the corrosion products of copper and lead. Such voltammetric responses, combined with X-ray fluorescence (XRF) spectroscopy experiments performed on the same set of coins, and complemented by focusing ion beam-field emission scanning electron microscope (FIB-FESEM) on silver coins from the 19th century, supported the hypothesis that two different metal sources were used in the former historical period and suggested that the coins were produced in three different mints. (C) 2016 Elsevier B.V. All rights reserve. es_ES
dc.description.sponsorship Financial support from the MINECO Projects CTQ2014-53736-C3-1-P and CTQ2014-53736-C3-2-P which are supported with ERDF funds is gratefully acknowledged. The authors are very grateful to the Polish Ministry of Science and Higher Education for partly financing the work presented in this paper through a grant within the framework of the National Program for the Development of the Humanities (Decision No. 0100/NPRH3/H12/82/2014) and also wish to thank Dr. Jose Luis Moya Lopez and Mr. Manuel Planes Insausti (Microscopy Service of the Universitat Politecnica de Valencia) for technical support. es_ES
dc.language Inglés es_ES
dc.publisher Elsevier es_ES
dc.relation.ispartof Microchemical Journal es_ES
dc.rights Reconocimiento - No comercial - Sin obra derivada (by-nc-nd) es_ES
dc.subject Voltammetry of immobilized particles es_ES
dc.subject Silver es_ES
dc.subject Copper es_ES
dc.subject Mediaeval Poland numismatic collections es_ES
dc.subject Long-term corrosion modeling es_ES
dc.subject.classification PINTURA es_ES
dc.title Electrochemical analysis of the first Polish coins using voltammetry of immobilized particles es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1016/j.microc.2016.07.020 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//CTQ2014-53736-C3-2-P/ES/APLICACION DE LAS TECNICAS NANOELECTROQUIMICAS Y BIOTECNOLOGICAS EN EL ESTUDIO Y CONSERVACION DEL PATRIMONIO EN METAL/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//CTQ2014-53736-C3-1-P/ES/APLICACION DE LAS TECNICAS NANOELECTROQUIMICAS Y BIOTECNOLOGIAS EN EL ESTUDIO Y CONSERVACION DEL PATRIMONIO EN METAL/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MNiSW//0100%2FNPRH3%2FH12%2F82%2F2014/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Conservación y Restauración de Bienes Culturales - Departament de Conservació i Restauració de Béns Culturals es_ES
dc.description.bibliographicCitation Doménech Carbó, A.; Del Hoyo Meléndez, JM.; Domenech Carbo, MT.; Piquero-Cilla, J. (2017). Electrochemical analysis of the first Polish coins using voltammetry of immobilized particles. Microchemical Journal. 130:47-55. https://doi.org/10.1016/j.microc.2016.07.020 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.1016/j.microc.2016.07.020 es_ES
dc.description.upvformatpinicio 47 es_ES
dc.description.upvformatpfin 55 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 130 es_ES
dc.relation.pasarela S\354684 es_ES
dc.contributor.funder European Regional Development Fund es_ES
dc.contributor.funder Ministerio de Economía y Competitividad es_ES
dc.contributor.funder Ministry of Science and Higher Education, Polonia es_ES


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