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Sequential determination of uranium and plutonium in soil and sediment samples by borate salts fusion

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Sequential determination of uranium and plutonium in soil and sediment samples by borate salts fusion

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Sáez-Muñoz, M.; Ortiz Moragón, J.; Martorell Alsina, SS.; Gómez-Arozamena, J.; Cearreta, A. (2020). Sequential determination of uranium and plutonium in soil and sediment samples by borate salts fusion. Journal of Radioanalytical and Nuclear Chemistry. 323(3):1167-1177. https://doi.org/10.1007/s10967-020-07028-5

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Título: Sequential determination of uranium and plutonium in soil and sediment samples by borate salts fusion
Autor: Sáez-Muñoz, Marina Ortiz Moragón, Josefina Martorell Alsina, Sebastián Salvador Gómez-Arozamena, J. Cearreta, A.
Entidad UPV: Universitat Politècnica de València. Departamento de Ingeniería Química y Nuclear - Departament d'Enginyeria Química i Nuclear
Fecha difusión:
Resumen:
[EN] This study describes a rapid method for sequential determination of uranium and plutonium isotopes in soil and sediment samples and its application to the study of Anthropocene sedimentary records. Different pretreatment ...[+]
Palabras clave: Fusion pretreatment , Uranium , Plutonium , Soil , Sediment , Borate salts
Derechos de uso: Reserva de todos los derechos
Fuente:
Journal of Radioanalytical and Nuclear Chemistry. (issn: 0236-5731 )
DOI: 10.1007/s10967-020-07028-5
Editorial:
Springer-Verlag
Versión del editor: https://doi.org/10.1007/s10967-020-07028-5
Código del Proyecto:
info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/RTI2018-095678-B-C21/ES/REGISTRO SEDIMENTARIO ANTROPOCENO EN LAS ZONAS COSTERA Y MARINA DEL NORTE DE IBERIA ATLANTICA/
info:eu-repo/grantAgreement/Eusko Jaurlaritza//IT976-16/
Agradecimientos:
The authors are grateful to the Universitat Politècnica de València for finantial support under the "Programa propio para la Formación de Personal Investigador (FPI) de la Universitat Politècnica de València - Subprograma ...[+]
Tipo: Artículo

References

Soppera N, Bossant M, Dupont E (2014) JANIS 4: an improved version of the NEA Java-based nuclear data information system. Nucl Data Sheets 120:294–296

UNSCEAR (2010) Sources and effects of ionizing radiation. Volume I: sources: report to the general assembly, scientific annexes A and B. UNSCEAR 2008 report. United Nations Scientific Committee on the Effects of Atomic Radiation. United Nations sales publication E.10.XI.3. United Nations, New York

Waters CN, Syvitski JPM, Gałuszka A, Hancock GJ, Zalasiewicz J, Cearreta A, Grinevald J, Jeandel C, McNeill JR, Summerhayes C, Barnosky A (2015) Can nuclear weapons fallout mark the beginning of the Anthropocene Epoch? Bull Atom Sci 71:46–57 [+]
Soppera N, Bossant M, Dupont E (2014) JANIS 4: an improved version of the NEA Java-based nuclear data information system. Nucl Data Sheets 120:294–296

UNSCEAR (2010) Sources and effects of ionizing radiation. Volume I: sources: report to the general assembly, scientific annexes A and B. UNSCEAR 2008 report. United Nations Scientific Committee on the Effects of Atomic Radiation. United Nations sales publication E.10.XI.3. United Nations, New York

Waters CN, Syvitski JPM, Gałuszka A, Hancock GJ, Zalasiewicz J, Cearreta A, Grinevald J, Jeandel C, McNeill JR, Summerhayes C, Barnosky A (2015) Can nuclear weapons fallout mark the beginning of the Anthropocene Epoch? Bull Atom Sci 71:46–57

IAEA (2015) The Fukushima Daiichi accident, technical radiological consequences, vol 4. International Atomic Energy Agency, Vienna

EPA (2012) EPA 402-R-12-006, radiological laboratory sample analysis guide for incident response—radionuclides in soil. U.S. Environmental Protection Agency, Montgomery

Mietelski JW, Wojtycza J, Zalewski M, Kapała J, Tomankiewicz E, Gaca P (2018) Plutonium and thorium isotopes in the bottom sediments of some Mazurian Lakes (Poland). J Radioanal Nucl Chem 318:2389–2399

Corcho-Alvarado JA, Diaz-Asencio M, Froidevaux P, Bochud F, Alonso-Hernández CM, Sanchez-Cabeza JA (2014) Dating young Holocene coastal sediments in tropical regions: use of fallout 239,240Pu as alternative chronostratigraphic marker. Quat Geochronol 22:1–10

Waters CN, Zalasiewicz J, Summerhayes C, Barnosky AD, Poirier C, Gałuszka A, Cearreta A, Edgeworth M, Ellis EC, Ellis M, Jeandel C, Leinfelder R, McNeill JR, Richter DDB, Steffen W, Syvitski J, Vidas D, Wagreich M, Williams M, Zhisheng A, Grinevald J, Odada E, Oreskes N, Wolfe AP (2016) The Anthropocene is functionally and stratigraphically distinct from the Holocene. Science 351(6269):aad2622

Zalasiewicz J, Waters CN, Summerhayes C, Wolfe AP, Barnosky AD, Cearreta A, Crutzen P, Ellis E, Fairchild IJ, Gałuszka A, Haff P, Hajdas I, Head MJ, Ivar do Sul JA, Jeandel C, Leinfelder R, McNeill JR, Neal C, Odada E, Oreskes N, Steffen W, Syvitski J, Vidas D, Wagreich M, Williams M (2017) The Working Group on the Anthropocene: summary of evidence and interim recommendations. Anthropocene 19:55–60

Qiao J, Hou X, Miró M, Roos P (2009) Determination of plutonium isotopes in waters and environmental solids: a review. Anal Chim Acta 652:66–84

Croudace I, Warwick P, Reading D, Russell B (2016) Recent contributions to the rapid screening of radionuclides in emergency responses and nuclear forensics. Trends Anal Chem 85:120–129

Casacuberta N, Lehritani M, Mantero J, Masqué P, Garcia-Orellana J, Garcia-Tenorio R (2012) Determination of U and Th α-emitters in NORM samples through extraction chromatography by using new and recycled UTEVA resins. Appl Radiat Isot 70:568–573

Lozano JC, Herranz M, Mosqueda F, Manjón G, Idoeta R, Quintana B, García-Tenorio R, Bolívar JP (2017) Low-level determination of Th-isotopes by alpha spectrometry. Part 2: evaluation of methods for dissolution of samples and for test sample preparation. J Radioanal Nucl Chem 314:2519–2529

Jurečič S, Benedik L, Planinšek P, Nečemer M, Kump P, Pihlar B (2014) Analysis of uranium in the insoluble residues after decomposition of soil samples by various techniques. Appl Radiat Isot 87:61–65

Luo M, Xing S, Yang Y, Song L, Ma Y, Wang Y, Dai X, Happel S (2018) Sequential analyses of actinides in large-size soil and sediment samples with total sample dissolution. J Environ Radioact 187:73–80

Sahli H, Röllin S, Putyrskaya V, Klemt E, Balsiger B, Burger M, Corcho Alvarado JA (2017) A procedure for the sequential determination of radionuclides in soil and sediment samples. J Radioanal Nucl Chem 314:2209–2218

Reading D, Croudace I, Warwick P, Britton R (2015) A rapid dissolution procedure to aid initial nuclear forensics investigations of chemically refractory compounds and particles prior to gamma spectrometry. Anal Chim Acta 900:1–9

IAEA (2009) IAEA/AQ/11A, procedure for the rapid determination of Pu isotopes and Am-241 in soil and sediment samples by alpha spectrometry, IAEA analytical quality in nuclear applications series no. 11. International Atomic Energy Agency, Vienna

Croudace I, Warwick P, Taylor R, Dee S (1998) Rapid procedure for plutonium and uranium determination in soils using a borate fusion followed by ion-exchange and extraction chromatography. Anal Chim Acta 371:217–225

Maxwell S, Culligan B, Hutchison J, McAlister D (2015) Rapid fusion method for the determination of Pu, Np, and Am in large soil samples. J Radioanal Nucl Chem 305:599–608

EPA (2014) EPA 402-R-14-004, rapid method for sodium hydroxide fusion of concrete and brick matrices prior to americium, plutonium, strontium, radium, and uranium analyses for environmental remediation following radiological incidents. U.S. Environmental Protection Agency, Montgomery

Maxwell S, Culligan B, Noyes G (2010) Rapid separation method for actinides in emergency soil samples. Radiochim Acta 98:793–800

Galindo C, Mougin L, Nourreddine A (2007) An improved radiochemical separation of uranium and thorium in environmental samples involving peroxide fusion. Appl Radiat Isot 65:9–16

EPA (2012) Rapid method for fusion of soil and soil-related matrices prior to americium, plutonium, and uranium analyses for environmental remediation following radiological incidents. U.S. Environmental Protection Agency, Montgomery

Mantero J, Lehritane M, Hurtado S, García-Tenorio R (2010) Radioanalytical determination of actinoids in refractory matrices by alkali fusion. J Radioanal Nucl Chem 286:557–563

Braysher E, Russell B, Woods S, García-Miranda M, Ivanov P, Bouchard B, Read D (2019) Complete dissolution of solid matrices using automated borate fusion in support of nuclear decommissioning and production of reference materials. J Radioanal Nucl Chem 321:183–196

Wang H, Ni Y, Zheng J, Huang Z, Xiao D, Aono T (2019) Low-temperature fusion using NH4HSO4 and NH4HF2 for rapid determination of Pu in soil and sediment samples. Anal Chim Acta 1050:71–79

Leorri E, Cearreta A, García-Artola A, Irabien MJ, Blake WH (2013) Relative sea-level rise in the Basque coast (N Spain): different environmental consequences on the coastal area. Ocean Coast Manag 77:3–13

Absi A (2005) Evolución del impacto radiactivo ambiental en la ría de Huelva tras el cambio en la gestión de los residuos de las industrias de producción deácido fosfórico. Doctoral thesis, Seville University

MARLAP (2004) Part II: chapter 13. Sample dissolution, (volume II), EPA 402-B-04-001B. In: Multi-agency radiological laboratory analytical protocols manual

Hallstadius L (1984) A method for the electrodeposition of actinides. Nucl Instrum Methods 223:266–267

Currie LA (1968) Limits for qualitative detection and quantitative determination. Application to radiochemistry. Anal Chem 40(3):586–593

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