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Catalytic Diastereo- and Enantioselective Synthesis of Tertiary Trifluoromethyl Carbinols through a Vinylogous Aldol Reaction of Alkylidenepyrazolones with Trifluoromethyl Ketones

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Catalytic Diastereo- and Enantioselective Synthesis of Tertiary Trifluoromethyl Carbinols through a Vinylogous Aldol Reaction of Alkylidenepyrazolones with Trifluoromethyl Ketones

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Carceller-Ferrer, L.; González Del Campo, A.; Vila, C.; Blay, G.; Muñoz Roca, MDC.; Pedro, JR. (2022). Catalytic Diastereo- and Enantioselective Synthesis of Tertiary Trifluoromethyl Carbinols through a Vinylogous Aldol Reaction of Alkylidenepyrazolones with Trifluoromethyl Ketones. Journal of Organic Chemistry. 87(7):4538-4549. https://doi.org/10.1021/acs.joc.1c02817

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Title: Catalytic Diastereo- and Enantioselective Synthesis of Tertiary Trifluoromethyl Carbinols through a Vinylogous Aldol Reaction of Alkylidenepyrazolones with Trifluoromethyl Ketones
Author: Carceller-Ferrer, Laura González del Campo, Aleix Vila, Carlos Blay, Gonzalo Muñoz Roca, María Del Carmen Pedro, José R.
UPV Unit: Universitat Politècnica de València. Escuela Técnica Superior de Ingeniería del Diseño - Escola Tècnica Superior d'Enginyeria del Disseny
Issued date:
Abstract:
[EN] A diastereo- and enantioselective organocatalyticaldol reaction between alkylidenepyrazolones and trifluoromethylketones leading to chiral tertiary alcohols bearing a trifluoromethylgroup is presented. The methodology ...[+]
Copyrigths: Reconocimiento (by)
Source:
Journal of Organic Chemistry. (issn: 0022-3263 )
DOI: 10.1021/acs.joc.1c02817
Publisher:
American Chemical Society
Publisher version: https://doi.org/10.1021/acs.joc.1c02817
Project ID:
info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/PID2020-116944GB-I00/ES/ESTRATEGIAS CATALITICAS ASIMETRICAS PARA LA SINTESIS DE NUEVAS ENTIDADES QUIMICAS QUIRALES CON POTENCIAL INTERES FARMACOLOGICO/
info:eu-repo/grantAgreement/MCIU//RYC-2016-20187//Ayudas para contratos Ramón y Cajal/
info:eu-repo/grantAgreement/CIUCSD//AICO%2F2020%2F68/
Thanks:
Financial support from Grant PID2020-116944GB funded by MCIN/AEI/10.13039/501100011033 and by "ERDF A way of making Europe" and AICO/2020/68 funded by Conselleria d'Innovacio, Universitat, Ciencia i Societat Digital ...[+]
Type: Artículo

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