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Synthesis of CuOx nanostructures in novel electrolytes under hydrodynamic conditions for photoelectrochemical applications

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Synthesis of CuOx nanostructures in novel electrolytes under hydrodynamic conditions for photoelectrochemical applications

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dc.contributor.author Sánchez-García, G. es_ES
dc.contributor.author Pérez-Calvo, A. es_ES
dc.contributor.author Fernández Domene, Ramón Manuel es_ES
dc.contributor.author Blasco-Tamarit, E. es_ES
dc.contributor.author Sánchez Tovar, Rita es_ES
dc.contributor.author Solsona, B. es_ES
dc.date.accessioned 2024-10-22T18:03:48Z
dc.date.available 2024-10-22T18:03:48Z
dc.date.issued 2023-10-17 es_ES
dc.identifier.issn 1477-9226 es_ES
dc.identifier.uri http://hdl.handle.net/10251/210696
dc.description.abstract [EN] In this work, CuOx (x = 1 and 2) nanostructures have been synthesized by electrochemical anodization in ethylene glycol based electrolytes using oxalic acid or NaF (with or without NaOH) as complexing agents. The influence of hydrodynamic conditions and time during anodization of copper have also been evaluated. A comprehensive morphological, structural, electrochemical and photoelectrochemical characterization of the nanostructures has been performed. The results revealed the convenient use of oxalic acid and 250 rpm for 5 minutes during electrochemical anodization to obtain homogeneous CuOx nanostructures formed by spheres with Cu2O as a predominant phase. Using this nanostructure as a photocathode for N2O photoelectron-reduction, almost 100% of N2O removal was achieved after 1 h, showing the improvement of the photoelectrochemical approach vs. the photo or the electro performance es_ES
dc.description.sponsorship The authors would like to acknowledge the Ministerio de Ciencia e Innovacion-Agencia Estatal de Investigacion through the projects PID2021-126235OB-C33 and TED2021-129555B-I00. The authors also thank the Generalitat Valenciana for CIAICO/2021/094, CIGRIS/2022/198, and CIGE/2022/166 and for the financial support (CIACIF/2021/010). es_ES
dc.language Inglés es_ES
dc.publisher The Royal Society of Chemistry es_ES
dc.relation.ispartof Dalton Transactions es_ES
dc.rights Reconocimiento - No comercial (by-nc) es_ES
dc.subject CuOx es_ES
dc.subject Nanostructures es_ES
dc.subject Electrolytes es_ES
dc.subject Photoelectrochemical applications es_ES
dc.subject.classification INGENIERIA QUIMICA es_ES
dc.title Synthesis of CuOx nanostructures in novel electrolytes under hydrodynamic conditions for photoelectrochemical applications es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1039/d3dt02017g es_ES
dc.relation.projectID info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2021-2023/PID2021-126235OB-C33/ES/ESTRATEGIAS CATALITICAS Y FOTOELECTROCATALITICAS PARA EVITAR LA EMISION DE N2O Y CO2 AL MEDIOAMBIENTE: VALORIZACION Y ELIMINACION/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/GVA//CIGRIS%2F2022%2F198/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/GVA//CIAICO%2F2021%2F094/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/GVA//CIGE%2F2022%2F166 / es_ES
dc.relation.projectID info:eu-repo/grantAgreement/GVA//CIACIF%2F2021%2F010/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/AEI//TED2021-129555B-I00//Proyectos Estratégicos Orientados a la Transición Ecológica y a la Transición Digital. Convocatoria 2021/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Escuela Técnica Superior de Ingenieros Industriales - Escola Tècnica Superior d'Enginyers Industrials es_ES
dc.description.bibliographicCitation Sánchez-García, G.; Pérez-Calvo, A.; Fernández Domene, RM.; Blasco-Tamarit, E.; Sánchez Tovar, R.; Solsona, B. (2023). Synthesis of CuOx nanostructures in novel electrolytes under hydrodynamic conditions for photoelectrochemical applications. Dalton Transactions. 52(40):14453-14464. https://doi.org/10.1039/d3dt02017g es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.1039/d3dt02017g es_ES
dc.description.upvformatpinicio 14453 es_ES
dc.description.upvformatpfin 14464 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 52 es_ES
dc.description.issue 40 es_ES
dc.identifier.pmid 37772605 es_ES
dc.relation.pasarela S\503711 es_ES
dc.contributor.funder Generalitat Valenciana es_ES
dc.contributor.funder Agencia Estatal de Investigación es_ES


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