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dc.contributor.author | Flores, M.F. | es_ES |
dc.contributor.author | García García, Pilar | es_ES |
dc.contributor.author | Garrido, N.M. | es_ES |
dc.contributor.author | Sanz, F. | es_ES |
dc.contributor.author | Díez, D. | es_ES |
dc.date.accessioned | 2013-07-03T08:54:06Z | |
dc.date.available | 2013-07-03T08:54:06Z | |
dc.date.issued | 2012 | |
dc.identifier.issn | 1600-5368 | |
dc.identifier.uri | http://hdl.handle.net/10251/30412 | |
dc.description.abstract | The title compound, C(14)H(19)NO(5)S, was prepared by nucleophilic addition of the lithium derivative of methyl-phenyl-sulfone to (3S,4R)-3,4-isopropyl-idene-dioxy-pyrroline 1-oxide. There are four mol-ecules in the asymmetric unit. The crystal structure determination confirms the configuration of the chiral centres as 2R,3S,4R. In the crystal, pairs of O-H¿N hydrogen bonds link the mol-ecules into dimers. | es_ES |
dc.language | Inglés | es_ES |
dc.publisher | International Union of Crystallography | es_ES |
dc.relation.ispartof | Acta Crystallographica Section E | es_ES |
dc.rights | Reconocimiento (by) | es_ES |
dc.title | (2R,3S,4R)-3,4-Isopropyl-idenedi-oxy-2-(phenyl-sulfonyl-meth-yl) pyrrolidin-1-ol | es_ES |
dc.type | Artículo | es_ES |
dc.identifier.doi | 10.1107/S1600536812033028 | |
dc.rights.accessRights | Abierto | es_ES |
dc.contributor.affiliation | Universitat Politècnica de València. Instituto Universitario Mixto de Tecnología Química - Institut Universitari Mixt de Tecnologia Química | es_ES |
dc.description.bibliographicCitation | Flores, M.; García García, P.; Garrido, N.; Sanz, F.; Díez, D. (2012). (2R,3S,4R)-3,4-Isopropyl-idenedi-oxy-2-(phenyl-sulfonyl-meth-yl) pyrrolidin-1-ol. Acta Crystallographica Section E. 68:2560-2560. doi:10.1107/S1600536812033028 | es_ES |
dc.description.accrualMethod | S | es_ES |
dc.relation.publisherversion | http://scripts.iucr.org/cgi-bin/paper?S1600536812033028 | es_ES |
dc.description.upvformatpinicio | 2560 | es_ES |
dc.description.upvformatpfin | 2560 | es_ES |
dc.type.version | info:eu-repo/semantics/publishedVersion | es_ES |
dc.description.volume | 68 | es_ES |
dc.relation.senia | 241254 | |
dc.identifier.pmid | 22904989 | en_EN |
dc.identifier.pmcid | PMC3415002 | en_EN |
dc.description.references | Bruker (2006). APEX2, SAINT and SADABS. Bruker AXS Inc., Madison, Wisconsin, USA. | es_ES |
dc.description.references | Chevrier, C., Le Nouën, D., Defoin, A., & Tarnus, C. (2011). Synthesis of 4-amino-4,5-dideoxy-l-lyxofuranose derivatives and their evaluation as fucosidase inhibitors. Carbohydrate Research, 346(10), 1202-1211. doi:10.1016/j.carres.2011.03.030 | es_ES |
dc.description.references | Flack, H. D. (1983). On enantiomorph-polarity estimation. Acta Crystallographica Section A Foundations of Crystallography, 39(6), 876-881. doi:10.1107/s0108767383001762 | es_ES |
dc.description.references | Flores, M. F., García, P., Garrido, N. M., Marcos, I. S., Sanz, F., & Díez, D. (2011). Sulfone chemistry for the synthesis of C-branched pyrrolidines. Tetrahedron: Asymmetry, 22(13), 1467-1472. doi:10.1016/j.tetasy.2011.08.001 | es_ES |
dc.description.references | Flores, M. F., Garcia, P., M. Garrido, N., Sanz, F., & Diez, D. (2011). (3R,4S)-3,4-Isopropylidenedioxy-5-phenylsulfonylmethyl-3,4-dihydro-2H-pyrrole 1-oxide. Acta Crystallographica Section E Structure Reports Online, 67(5), o1115-o1115. doi:10.1107/s1600536811010737 | es_ES |
dc.description.references | Flores, M. F., Núñez, M. G., Moro, R. F., Garrido, N. M., Marcos, I. S., Iglesias, E. F., … Díez, D. (2010). Synthesis of a New Chiral Pyrrolidine. Molecules, 15(3), 1501-1512. doi:10.3390/molecules15031501 | es_ES |
dc.description.references | Lattanzi, A. (2009). α,α-Diarylprolinols: bifunctional organocatalysts for asymmetric synthesis. Chemical Communications, (12), 1452. doi:10.1039/b900098d | es_ES |
dc.description.references | Li, X., Qin, Z., Wang, R., Chen, H., & Zhang, P. (2011). Stereoselective synthesis of novel C-azanucleoside analogues by microwave-assisted nucleophilic addition of sugar-derived cyclic nitrones. Tetrahedron, 67(10), 1792-1798. doi:10.1016/j.tet.2011.01.038 | es_ES |
dc.description.references | List, B. (2007). Introduction: Organocatalysis. Chemical Reviews, 107(12), 5413-5415. doi:10.1021/cr078412e | es_ES |
dc.description.references | MacMillan, D. W. C. (2008). The advent and development of organocatalysis. Nature, 455(7211), 304-308. doi:10.1038/nature07367 | es_ES |
dc.description.references | Macrae, C. F., Edgington, P. R., McCabe, P., Pidcock, E., Shields, G. P., Taylor, R., … van de Streek, J. (2006). Mercury: visualization and analysis of crystal structures. Journal of Applied Crystallography, 39(3), 453-457. doi:10.1107/s002188980600731x | es_ES |
dc.description.references | Mielgo, A., & Palomo, C. (2008). α,α-Diarylprolinol Ethers: New Tools for Functionalization of Carbonyl Compounds. Chemistry – An Asian Journal, 3(6), 922-948. doi:10.1002/asia.200700417 | es_ES |
dc.description.references | Panday, S. K. (2011). Advances in the chemistry of proline and its derivatives: an excellent amino acid with versatile applications in asymmetric synthesis. Tetrahedron: Asymmetry, 22(20-22), 1817-1847. doi:10.1016/j.tetasy.2011.09.013 | es_ES |
dc.description.references | Pellissier, H. (2007). Asymmetric organocatalysis. Tetrahedron, 63(38), 9267-9331. doi:10.1016/j.tet.2007.06.024 | es_ES |
dc.description.references | Sheldrick, G. M. (2007). A short history ofSHELX. Acta Crystallographica Section A Foundations of Crystallography, 64(1), 112-122. doi:10.1107/s0108767307043930 | es_ES |