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A statistical design of experiments for optimizing the MALDI-TOF-MS sample preparation of polymers. An application in the assessment of the thermo-mechanical degradation mechanisms of poly (ethylene terephthalate)

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A statistical design of experiments for optimizing the MALDI-TOF-MS sample preparation of polymers. An application in the assessment of the thermo-mechanical degradation mechanisms of poly (ethylene terephthalate)

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Badía Valiente, JD.; Strömberg, EM.; Ribes Greus, MD.; Karlsson, S. (2011). A statistical design of experiments for optimizing the MALDI-TOF-MS sample preparation of polymers. An application in the assessment of the thermo-mechanical degradation mechanisms of poly (ethylene terephthalate). ANALYTICA CHIMICA ACTA. 692(1):85-95. doi:10.1016/j.aca.2011.02.063

Por favor, use este identificador para citar o enlazar este ítem: http://hdl.handle.net/10251/30823

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Título: A statistical design of experiments for optimizing the MALDI-TOF-MS sample preparation of polymers. An application in the assessment of the thermo-mechanical degradation mechanisms of poly (ethylene terephthalate)
Autor:
Entidad UPV: Universitat Politècnica de València. Departamento de Máquinas y Motores Térmicos - Departament de Màquines i Motors Tèrmics
Universitat Politècnica de València. Instituto de Tecnología de Materiales - Institut de Tecnologia de Materials
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Resumen:
[EN] The sample preparation procedure for MALDI-TOF MS of polymers is addressed in this study by the application of a statistical Design of Experiments (DoE). Industrial poly (ethylene terephthalate) (PET) was chosen as ...[+]
Palabras clave: Design of Experiments , Mass spectrometry , Matrix-assisted laser desorption/ionization time-of-flight , Poly (ethylene terephthalate) , Recycling , Thermo-mechanical degradation , Cationization , Degradation mechanism , Glycol units , Injection cycles , MALDI TOF MS , Matrix , Mechanical recycling , Multiple processing , Potential reactions , Quality parameters , Sample preparation , Sample preparation procedure , Signal to noise , Statistical design of experiments , Degradation , Desorption , Ethers , Ethylene , Glycols , Inductively coupled plasma , Mechanisms , Oligomers , Polymers , Signal to noise ratio , Polyethylene terephthalates , Dithranol , Polyethylene terephthalate , Article , Controlled study , Degradation kinetics , Hydrolysis , Matrix assisted laser desorption ionization time of flight mass spectrometry , Priority journal , Process optimization , Signal noise ratio , Simulation , Transesterification
Derechos de uso: Cerrado
Fuente:
ANALYTICA CHIMICA ACTA. (issn: 0003-2670 )
DOI: 10.1016/j.aca.2011.02.063
Editorial:
ELSEVIER SCIENCE BV
Versión del editor: http://dx.doi.org/10.1016/j.aca.2011.02.063
Agradecimientos:
The authors would like to acknowledge the Spanish Ministry of Science and Innovation for the financial support through the Research Project UPOVCE-3E-013. The Spanish Ministry for Education is acknowledged for the concession ...[+]
Tipo: Artículo

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