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Assessing the MALDI-TOF MS sample preparation procedure to analyze the influence of thermo-oxidative ageing and thermo-mechanical degradation on poly (Lactide)

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Assessing the MALDI-TOF MS sample preparation procedure to analyze the influence of thermo-oxidative ageing and thermo-mechanical degradation on poly (Lactide)

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J.D. Badia; Strömberg, EM.; Ribes Greus, MD.; Karlsson, S. (2011). Assessing the MALDI-TOF MS sample preparation procedure to analyze the influence of thermo-oxidative ageing and thermo-mechanical degradation on poly (Lactide). EUROPEAN POLYMER JOURNAL. 47(7):1416-1428. doi:10.1016/j.eurpolymj.2011.05.001.

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Título: Assessing the MALDI-TOF MS sample preparation procedure to analyze the influence of thermo-oxidative ageing and thermo-mechanical degradation on poly (Lactide)
Autor:
Entidad UPV: Universitat Politècnica de València. Departamento de Máquinas y Motores Térmicos - Departament de Màquines i Motors Tèrmics
Fecha difusión:
Resumen:
Multiple processing by means of successive injection cycles was used to simulate the thermo-mechanical degradation effects on the oligomeric distribution of PLA under mechanical recycling. Likewise, an accelerated thermal ...[+]
Palabras clave: Design of Experiments (DoE) , Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry (MALDI-TOF MS) , Polylactide (PLA) , Thermo-mechanical degradation , Thermo-oxidative ageing , Analytes , Cationization , Deep inspection , Degradation mechanism , Injection cycles , MALDI TOF MS , Matrix , Matrix-assisted laser desorption/ionization-time-of-flight mass spectrometry , Mechanical recycling , Multiple processing , Poly(lactide) , Polylactides , Repeating unit , Sample preparation procedure , Signal to noise , Statistical design of experiments , Transesterifications , Design of experiments , Desorption , Experiments , Glass lasers , Glass transition , Mass spectrometry , Mechanisms , Oligomers , Signal to noise ratio , Degradation
Derechos de uso: Cerrado
Fuente:
EUROPEAN POLYMER JOURNAL. (issn: 0014-3057 )
DOI: 10.1016/j.eurpolymj.2011.05.001
Editorial:
Elsevier
Versión del editor: http://dx.doi.org/10.1016/j.eurpolymj.2011.05.001
Patrocinador:
Spanish Ministry of Science and Innovation [UPOVCE-3E-013]
Spanish Ministry for Education
Royal Institute of Technology (KTH, Sweden)
Universitat Politecnica de Valencia (UPV, Spain)
Tipo: Artículo

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