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Assessment of Parameters Influencing fiber characteristics of chitosan nanofiber membrane to optimize fiber mat productioi

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Assessment of Parameters Influencing fiber characteristics of chitosan nanofiber membrane to optimize fiber mat productioi

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dc.contributor.author Areias, A.C. es_ES
dc.contributor.author Gómez-Tejedor, José Antonio es_ES
dc.contributor.author Sencadas, V. es_ES
dc.contributor.author Alio, J. es_ES
dc.contributor.author Gómez Ribelles, José Luís es_ES
dc.contributor.author Lanceros-Mendez, S. es_ES
dc.date.accessioned 2014-09-26T12:14:28Z
dc.date.available 2014-09-26T12:14:28Z
dc.date.issued 2012-06
dc.identifier.issn 0032-3888
dc.identifier.uri http://hdl.handle.net/10251/40304
dc.description.abstract Electrospun chitosan nanofiber mats have been obtained using chitosan solutions in a mixture of trifluoroacetic acid and dichloromethane. The relationship between processing parameters (solvent composition, polymer concentration in the solution, feeding rate, applied voltage, traveling distance between the needle, and the collector) and fiber morphology was studied. Taguchi's methodology was followed to determine which parameters have the strongest influence on mean fiber diameter and fiber homogeneity. Chitosan nanofibers obtained with this procedure were water soluble due to the protonation of amine side groups but were successfully neutralized by immersion in calcium carbonate solutions. It was established that fiber diameter is mainly determined by the solution concentration and the distance from the needle to the collector while other parameters have less influence. The set of parameters that produce the thinnest fibers were a concentration of 8 wt%, a TFA/DCM ratio of 80:20 (v/v%), a voltage of 30 kV, a flow rate of 6.0 mL/h, a gap distance of 10 cm, using a needle diameter of 0.5, allowing to produce randomly oriented mats with a mean fiber thickness of 66 nm. © 2012 Society of Plastics Engineers. es_ES
dc.description.sponsorship Contract grant sponsor: Portuguese Foundation for Science and Technology (FCT); contract grant number: NANO/NMed-SD/0156/2007; Contract grant sponsor: FCT; contract grant number: SFRH/BPD/63148/2009; Contract grant sponsor: Spanish Ministry of Science and Innovation; contract grant number: MAT2010-21611-C03-01; Contract grant sponsor: Programa Nacional de Internacionalizacion de la I+D; contract grant number: EUI2008-00126; Contract grant sponsors: Regenerative Medicine collaboration agreement from the Conselleria de Sanidad (Generalitat Valenciana), and the Instituto de Salud Carlos III (Ministry of Science and Innovation); Contract grant sponsors: Spanish Ministry of Science and Innovation, Centro para el Desarrollo Tecnologico Industrial (CDTI), CENIT: "Customized Eye Care'' and CeyeC; contract grant number: CEN-20091021; Contract grant sponsor: The translation of this paper was funded by the Universitat Politecnica de Valencia, Spain. en_EN
dc.language Inglés es_ES
dc.publisher Wiley es_ES
dc.relation.ispartof Polymer Engineering and Science es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Applied voltages es_ES
dc.subject Carbonate solutions es_ES
dc.subject Chitosan nanofibers es_ES
dc.subject Chitosan solution es_ES
dc.subject Electrospuns es_ES
dc.subject Feeding rate es_ES
dc.subject Fiber characteristics es_ES
dc.subject Fiber diameters es_ES
dc.subject Chitin es_ES
dc.subject Biomaterials es_ES
dc.subject Regeneration es_ES
dc.subject.classification FISICA APLICADA es_ES
dc.subject.classification MAQUINAS Y MOTORES TERMICOS es_ES
dc.title Assessment of Parameters Influencing fiber characteristics of chitosan nanofiber membrane to optimize fiber mat productioi es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1002/pen.23070
dc.relation.projectID info:eu-repo/grantAgreement/MICINN//MAT2010-21611-C03-01/ES/MATERIALES BIOESTABLES Y BIOREABSORBIBLES A LARGO PLAZO COMO SOPORTES MACROPOROSOS PARA LA REGENERACION DEL CARTILAGO ARTICULAR/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/FCT/5876-PPCDTI/109368/PT/“Smart joint implants using bionanocomposites-(SIMBIO)”/
dc.relation.projectID info:eu-repo/grantAgreement/MICINN//EUI2008-00126/ES/SMART JOINT IMPLANTS USING BIONANOCOMPOSITES/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/FCT/SFRH/SFRH%2FBPD%2F63148%2F2009/PT/ELECTROACTIVE MATERIALS BASED POROUS MEMBRANES AND SCAFFOLDS FOR BIOMEDICAL APPLICATIONS/
dc.relation.projectID info:eu-repo/grantAgreement/CIBER-BBN//00028336 SFPECEPP/ES/Customized Eye Care-Oftalmologia personalizada/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MICINN//CEN-20091021/ES/CUSTOMATIZED EYE CARE. OFTALMOLOGÍA PERSONALIZADA Y MÍNIMAMENTE INVASIVA/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Física Aplicada - Departament de Física Aplicada es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Termodinámica Aplicada - Departament de Termodinàmica Aplicada es_ES
dc.contributor.affiliation Universitat Politècnica de València. Centro de Biomateriales e Ingeniería Tisular - Centre de Biomaterials i Enginyeria Tissular es_ES
dc.description.bibliographicCitation Areias, A.; Gómez-Tejedor, JA.; Sencadas, V.; Alio, J.; Gómez Ribelles, JL.; Lanceros-Mendez, S. (2012). Assessment of Parameters Influencing fiber characteristics of chitosan nanofiber membrane to optimize fiber mat productioi. Polymer Engineering and Science. 52(6):1293-1300. https://doi.org/10.1002/pen.23070 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://dx.doi.org/10.1002/pen.23070 es_ES
dc.description.upvformatpinicio 1293 es_ES
dc.description.upvformatpfin 1300 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 52 es_ES
dc.description.issue 6 es_ES
dc.relation.senia 232036
dc.contributor.funder Centro de Investigación Biomédica en Red en Bioingeniería, Biomateriales y Nanomedicina es_ES
dc.contributor.funder Centro para el Desarrollo Tecnológico Industrial es_ES
dc.contributor.funder Generalitat Valenciana es_ES
dc.contributor.funder Instituto de Salud Carlos III es_ES
dc.contributor.funder Universitat Politècnica de València es_ES
dc.contributor.funder Fundação para a Ciência e a Tecnologia, Portugal
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