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Control parameters on the fabrication of ZnO hollow nanocolumns

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Control parameters on the fabrication of ZnO hollow nanocolumns

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dc.contributor.author Cembrero Cil, Jesús es_ES
dc.contributor.author Busquets Mataix, David Jerónimo es_ES
dc.contributor.author Rayón Encinas, Emilio es_ES
dc.contributor.author Pascual Muñoz, Manuel es_ES
dc.contributor.author Pérez Puig, Miguel Angel es_ES
dc.contributor.author Marí Soucase, Bernabé es_ES
dc.date.accessioned 2015-05-22T06:10:29Z
dc.date.available 2015-05-22T06:10:29Z
dc.date.issued 2013-02
dc.identifier.issn 1369-8001
dc.identifier.uri http://hdl.handle.net/10251/50669
dc.description.abstract [EN] The present work reports on the fabrication of hollow ZnO nanocolumns by a sequential combination of electrochemical deposition, chemical attack and regeneration. Initially, ZnO nanocolumns were deposited in two different substrates, namely Fluor Tin Oxide and Indium Tin Oxide. In a further step, a statistical analysis on the most influencing control parameters in the dissolution stage to produce the hollow ZnO nanowires on the FTO substrates was carried out. The control variables considered were electrolyte concentration, dissolution time and temperature, whereas the output variable was the percentage of the hollow nanocolumns obtained. The statistical analysis consisted of a two-level factorial design of experiments on three variables, therefore involving a series of 8 experiments. An analysis of variance (ANOVA) on the results was also carried out. The results showed that all the control variables were significant, the most important being the dissolution time. es_ES
dc.description.sponsorship This work was supported by the Spanish Government through MCINN Grant MAT2009-14625-C03-03, Generalitat Valenciana programme PROMETEO/2009/063 and European Commission through NanoCIS project FP7-PEOPLE-2010-IRSES (ref. 269279). Technical support given to the authors by the Servei de Microscopia at the Universitat Politecnica de Valencia (Spain) is greatly acknowledged. en_EN
dc.language Inglés es_ES
dc.publisher Elsevier es_ES
dc.relation info:eu-repo/grantAgreement/Generalitat Valenciana//PROMETEO09%2F2009%2F063/ES/Investigaciones en diseño para la fabricación y producción automatizada/ es_ES
dc.relation info:eu-repo/grantAgreement/MICINN//MAT2009-14625-C03-03/ES/Diseño, Sintesis Y Caracterizacion De Materiales Fotovoltaicos Avanzados De Alta Eficiencia/ es_ES
dc.relation.ispartof Materials Science in Semiconductor Processing es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject ANOVA es_ES
dc.subject two-level factorial design es_ES
dc.subject Hollow ZnO nanocolumns es_ES
dc.subject Semiconducting II–VI materials es_ES
dc.subject Zinc compounds es_ES
dc.subject Oxides es_ES
dc.subject Growth from solutions es_ES
dc.subject Nanostructures es_ES
dc.subject Electron Microscopy Service of the UPV es_ES
dc.subject.classification CIENCIA DE LOS MATERIALES E INGENIERIA METALURGICA es_ES
dc.subject.classification FISICA APLICADA es_ES
dc.title Control parameters on the fabrication of ZnO hollow nanocolumns es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1016/j.mssp.2012.04.014
dc.relation.projectID info:eu-repo/grantAgreement/EC/FP7/269279/EU/Development of a new generation of CIGS-based solar cells/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Ingeniería Mecánica y de Materiales - Departament d'Enginyeria Mecànica i de Materials es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Física Aplicada - Departament de Física Aplicada es_ES
dc.description.bibliographicCitation Cembrero Cil, J.; Busquets Mataix, DJ.; Rayón Encinas, E.; Pascual Muñoz, M.; Pérez Puig, MA.; Marí Soucase, B. (2013). Control parameters on the fabrication of ZnO hollow nanocolumns. Materials Science in Semiconductor Processing. 16:211-216. https://doi.org/10.1016/j.mssp.2012.04.014 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://www.sciencedirect.com/science/article/pii/S1369800112000595 es_ES
dc.description.upvformatpinicio 211 es_ES
dc.description.upvformatpfin 216 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 16 es_ES
dc.relation.senia 228619
dc.contributor.funder European Commission
dc.contributor.funder Ministerio de Ciencia e Innovación
dc.contributor.funder Generalitat Valenciana


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