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Monitoring stabilizing procedures of archaeological iron using electrochemical impedance spectroscopy

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Monitoring stabilizing procedures of archaeological iron using electrochemical impedance spectroscopy

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dc.contributor.author Domenech Carbo, Antonio es_ES
dc.contributor.author Lastras Pérez, Montserrat es_ES
dc.contributor.author Rodríguez Calás, Francisco es_ES
dc.contributor.author Cano, Emilio es_ES
dc.contributor.author Piquero Cilla, Juan es_ES
dc.contributor.author Osete Cortina, Laura es_ES
dc.date.accessioned 2015-07-17T08:10:01Z
dc.date.available 2015-07-17T08:10:01Z
dc.date.issued 2013
dc.identifier.issn 1432-8488
dc.identifier.uri http://hdl.handle.net/10251/53382
dc.description.abstract A methodology for monitoring washing procedures applied to stabilize archaeological iron is described. It is based on the combination of voltammetry of microparticles (VMP) with electrochemical impedance spectroscopy (EIS). A semiempirical approach is used where the impedances at low and high frequencies were related with the fraction areas of passive and corrosion layers generated during the stabilizing treatment, the thickness, and the porosity of the corrosion layer. The variation of such parameters with the time of washing was determined from EIS data for four types of desalination procedures using concentrated NaOH and/or Na2SO3 aqueous solutions on archaeological iron artifacts. After 2 months of treatment, EIS data indicate that an essentially identical stable state was attained in all cases, as confirmed by the formation of a passive magnetite layer identified in VMP measurements while the rate of variation of corroded surface and porosity at short washing times varied significantly from one stabilization procedure to another. es_ES
dc.description.sponsorship Financial support from the MEC Project CTQ2011-28079-CO3-02 which is supported with ERDF funds is gratefully acknowledged. en_EN
dc.language Inglés es_ES
dc.publisher Springer Verlag (Germany) es_ES
dc.relation.ispartof Journal of Solid State Electrochemistry es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Archaelogical iron es_ES
dc.subject Desalinationmethods es_ES
dc.subject Electrochemical impedance spectroscopy es_ES
dc.subject Voltammetry of microparticles es_ES
dc.subject Conservation restoration es_ES
dc.subject.classification PINTURA es_ES
dc.title Monitoring stabilizing procedures of archaeological iron using electrochemical impedance spectroscopy es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1007/s10008-013-2232-y
dc.relation.projectID info:eu-repo/grantAgreement/MICINN//CTQ2011-28079-C03-02/ES/DESARROLLO DE METODOS NANOELECTROQUIMICOS DE ANALSISIS DE OBRAS PICTORICAS BASADOS EN "ONE-TOUCH", "LAYER-BY-LAYER" VOLTAMPEROMETRIA DE MICRO%2FNANOPARTICULAS Y MICROSCOPIA ELEC/
dc.rights.accessRights Cerrado es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Conservación y Restauración de Bienes Culturales - Departament de Conservació i Restauració de Béns Culturals es_ES
dc.contributor.affiliation Universitat Politècnica de València. Instituto Universitario de Restauración del Patrimonio - Institut Universitari de Restauració del Patrimoni es_ES
dc.description.bibliographicCitation Domenech Carbo, A.; Lastras Pérez, M.; Rodríguez Calás, F.; Cano, E.; Piquero Cilla, J.; Osete Cortina, L. (2013). Monitoring stabilizing procedures of archaeological iron using electrochemical impedance spectroscopy. Journal of Solid State Electrochemistry. 18(2):399-409. https://doi.org/10.1007/s10008-013-2232-y es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://dx.doi.org/10.1007/s10008-013-2232-y es_ES
dc.description.upvformatpinicio 399 es_ES
dc.description.upvformatpfin 409 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 18 es_ES
dc.description.issue 2 es_ES
dc.relation.senia 258602
dc.identifier.eissn 1433-0768
dc.contributor.funder Ministerio de Ciencia e Innovación
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