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Development of a photoinduced chemiluminescent method for the determination of the herbicide quinmerac in water

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Development of a photoinduced chemiluminescent method for the determination of the herbicide quinmerac in water

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dc.contributor.author Catalá-Icardo, Mónica es_ES
dc.contributor.author López Paz, José Luis es_ES
dc.contributor.author Blázquez Pérez, Juncal es_ES
dc.date.accessioned 2016-01-26T18:46:51Z
dc.date.available 2016-01-26T18:46:51Z
dc.date.issued 2015-10
dc.identifier.issn 0003-7028
dc.identifier.uri http://hdl.handle.net/10251/60201
dc.description This paper was published in APPLIED SPECTROSCOPY and is made available as an electronic reprint with the permission of OSA. The paper can be found at the following URL on the OSA website: http://dx.doi.org/10.1366/14-07791 . Systematic or multiple reproduction or distribution to multiple locations via electronic or other means is prohibited and is subject to penalties under law. es_ES
dc.description.abstract A new, simple and sensitive method, based on photoinduced chemiluminescence, was developed for the determination of quinmerac. The photoproduct, obtained after UV irradiation in basic medium, was mixed with sodium sulfite (sensitizer), and Ce(IV) (oxidant) in acid medium. A wide linear dynamic range (2-600 ng mL-1) and a limit of detection of 0.6 ng mL-1 were obtained without any pretreatment (0.08 ng mL-1 after solid phase extraction). The determination was performed using a flow injection manifold, which allowed a high throughput (144 h-1). The inter-day reproducibility was 5.6% (n=5), and the intra-day repeatability was 3.9 and 2.9% for 20 and 200 ng mL-1 of quinmerac, respectively (n=21). Finally, the method was applied to surface and ground waters with recoveries ranging from 78.1 to 94.5%. es_ES
dc.description.sponsorship The authors thank the Ministerio de Educacion y Ciencia from Spain and FEDER for financial support, Project CTM2006-11991. en_EN
dc.language Inglés es_ES
dc.publisher SAGE Publications (UK and US) es_ES
dc.relation.ispartof Applied Spectroscopy es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Quinmerac es_ES
dc.subject Photoinduced chemiluminescence es_ES
dc.subject Pesticides es_ES
dc.subject Flow injection es_ES
dc.subject Water es_ES
dc.subject.classification QUIMICA ANALITICA es_ES
dc.title Development of a photoinduced chemiluminescent method for the determination of the herbicide quinmerac in water es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1366/14-07791
dc.relation.projectID info:eu-repo/grantAgreement/MEC//CTM2006-11991/ES/DESARROLLO DE METODOS SENCILLOS EN FLUJO CONTINUO CON DETECCION QUIMIOLUMINISCENTE APLICADOS AL CONTROL DE PLAGUICIDAS EN LOS CULTIVOS DE CITRICOS/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Química - Departament de Química es_ES
dc.contributor.affiliation Universitat Politècnica de València. Instituto de Investigación para la Gestión Integral de Zonas Costeras - Institut d'Investigació per a la Gestió Integral de Zones Costaneres es_ES
dc.description.bibliographicCitation Catalá-Icardo, M.; López Paz, JL.; Blázquez Pérez, J. (2015). Development of a photoinduced chemiluminescent method for the determination of the herbicide quinmerac in water. Applied Spectroscopy. 69(10):1199-1204. https://doi.org/10.1366/14-07791 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://dx.doi.org/10.1366/14-07791 es_ES
dc.description.upvformatpinicio 1199 es_ES
dc.description.upvformatpfin 1204 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 69 es_ES
dc.description.issue 10 es_ES
dc.relation.senia 296421 es_ES
dc.contributor.funder Ministerio de Educación y Ciencia es_ES
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