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Contact probe electrochemical characterization and metal speciation of silver LLDPE nanocomposite films

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Contact probe electrochemical characterization and metal speciation of silver LLDPE nanocomposite films

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dc.contributor.author Domínguez, Irene es_ES
dc.contributor.author Domenech Carbo, Antonio es_ES
dc.contributor.author Cerisuelo Ferriols, Josep Pascual es_ES
dc.contributor.author López Carballo, Gracia es_ES
dc.contributor.author Hernandez Muñoz, Maria Pilar es_ES
dc.contributor.author GAVARA CLEMENTE, RAFAEL es_ES
dc.date.accessioned 2017-04-20T06:30:33Z
dc.date.available 2017-04-20T06:30:33Z
dc.date.issued 2014-08
dc.identifier.issn 1432-8488
dc.identifier.uri http://hdl.handle.net/10251/79832
dc.description.abstract [EN] A contact probe methodology, based on the voltammetry of immobilized microparticle approach, is used for characterizing silver species present in linear low density polyethylene (LLDPE) films with different Ag(I)/Ag(0) ratios and silver nanoparticle features usable as food contact polymers. The films displayed characteristic voltammetric features in contact with aqueous acetate buffer, in particular signals for the stripping oxidation of nanoparticulate Ag systems. Significant differences between the studied films were also observed by means of electrochemical impedance spectroscopy and detected at the nanoscopic scale using electrochemical scanning microscopy. Differences in optical and thermal properties of the studied films are associated with the presence of silver nanoparticles. The silver oxidation state as well as nanoparticle size also had influence on the oxidative resistance of the LLDPE films; indeed, films containing cationic silver showed the lowest oxidation induction time value. es_ES
dc.description.sponsorship The authors wish to thank the Spanish Ministry of Science and Innovation for financial support through projects INGENIO-CONSOLIDER CSD2007-00063, AGL-2012-39920-C03-01, and CTQ2011-28079-C03-02, supported by ERDF funds, and Mr. Tim Swillens (translation services). I. D. thanks the CSIC for the postdoctoral contract concession.
dc.language Inglés es_ES
dc.publisher Springer Verlag (Germany) es_ES
dc.relation.ispartof Journal of Solid State Electrochemistry es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Solid state electrochemistry es_ES
dc.subject Polyethylene film es_ES
dc.subject Silver es_ES
dc.subject Speciation es_ES
dc.subject.classification TECNOLOGIA DE ALIMENTOS es_ES
dc.title Contact probe electrochemical characterization and metal speciation of silver LLDPE nanocomposite films es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1007/s10008-014-2453-8
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//AGL2012-39920-C03-01/ES/NUEVOS SISTEMAS POLIMERICOS ACTIVOS PARA EL ENVASADO DE ALIMENTOS SENSIBLES AL DETERIORO MICROBIOLOGICO Y OXIDATIVO/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MICINN//CTQ2011-28079-C03-02/ES/DESARROLLO DE METODOS NANOELECTROQUIMICOS DE ANALSISIS DE OBRAS PICTORICAS BASADOS EN "ONE-TOUCH", "LAYER-BY-LAYER" VOLTAMPEROMETRIA DE MICRO%2FNANOPARTICULAS Y MICROSCOPIA ELEC/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MEC//CSD2007-00063/ES/Nuevos Ingredientes de Alimentos Funcionales para Mejorar la Salud/
dc.rights.accessRights Cerrado es_ES
dc.contributor.affiliation Universitat Politècnica de València. Escuela Técnica Superior de Ingeniería Agronómica y del Medio Natural - Escola Tècnica Superior d'Enginyeria Agronòmica i del Medi Natural es_ES
dc.description.bibliographicCitation Domínguez, I.; Domenech Carbo, A.; Cerisuelo Ferriols, JP.; López Carballo, G.; Hernandez Muñoz, MP.; Gavara Clemente, R. (2014). Contact probe electrochemical characterization and metal speciation of silver LLDPE nanocomposite films. Journal of Solid State Electrochemistry. 18(8):2099-2110. https://doi.org/10.1007/s10008-014-2453-8 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://doi.org/10.1007/s10008-014-2453-8 es_ES
dc.description.upvformatpinicio 2099 es_ES
dc.description.upvformatpfin 2110 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 18 es_ES
dc.description.issue 8 es_ES
dc.relation.senia 274654 es_ES
dc.identifier.eissn 1433-0768
dc.contributor.funder Ministerio de Educación y Ciencia
dc.contributor.funder Ministerio de Economía y Competitividad es_ES
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