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Microwave synthesis of microstructured and nanostructured metal chalcogenides from elemental precursors in phosphonium ionic liquids

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Microwave synthesis of microstructured and nanostructured metal chalcogenides from elemental precursors in phosphonium ionic liquids

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Nombre: K. Ding;H. Lu;Y. ...
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dc.contributor.author Ding, Kunlun es_ES
dc.contributor.author Lu, Hong es_ES
dc.contributor.author Zhang, Yichi. es_ES
dc.contributor.author Snedaker, Matthew L. es_ES
dc.contributor.author Liu, Deyu es_ES
dc.contributor.author Maciá-Agulló, J.A. es_ES
dc.contributor.author Stucky, Galen D. es_ES
dc.date.accessioned 2017-07-03T08:58:39Z
dc.date.issued 2014-11-05
dc.identifier.issn 0002-7863
dc.identifier.uri http://hdl.handle.net/10251/84326
dc.description.abstract [EN] We describe a general approach for the synthesis of micro-/nanostructured metal chalcogenides from elemental precursors. The excellent solubility of sulfur, selenium, and tellurium in phosphonium ionic liquids promotes fast reactions between chalcogens and various metal powders upon microwave heating, giving crystalline products. This approach is green, universal, and scalable. es_ES
dc.description.sponsorship This research was supported by the Center for Energy Efficient Materials, an Energy Frontier Research Center funded by the U.S. Department of Energy, Office of Science, Basic Energy Sciences under Award No. DE-SC0001009, and by the National Science Foundation (DMR 0805148). We thank Cytec Industries Inc. for kindly providing us several types of phosphonium ionic liquids without cost. The MRL Shared Experimental Facilities are supported by the MRSEC Program of the NSF under Award No. DMR 1121053(a member of the NSF-funded Materials Research Facilities Network, www.mrfn.org).
dc.language Inglés es_ES
dc.publisher American Chemical Society es_ES
dc.relation.ispartof Journal of the American Chemical Society es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Microwave synthesis es_ES
dc.subject Nanostructured metals es_ES
dc.subject Phosphonium ionic liquid es_ES
dc.subject.classification QUIMICA ORGANICA es_ES
dc.title Microwave synthesis of microstructured and nanostructured metal chalcogenides from elemental precursors in phosphonium ionic liquids es_ES
dc.type Artículo es_ES
dc.embargo.lift 10000-01-01
dc.embargo.terms forever es_ES
dc.identifier.doi 10.1021/ja508628q
dc.relation.projectID info:eu-repo/grantAgreement/DOE//DE-SC0001009/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/NSF//0805148/US/Chemical Methods to Control Charge Transfer at Nanoscale Interfaces/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/NSF//1121053/US/Center of Excellence for Materials Research and Innovation at UCSB/ es_ES
dc.rights.accessRights Cerrado es_ES
dc.contributor.affiliation Universitat Politècnica de València. Instituto Universitario Mixto de Tecnología Química - Institut Universitari Mixt de Tecnologia Química es_ES
dc.description.bibliographicCitation Ding, K.; Lu, H.; Zhang, Y.; Snedaker, ML.; Liu, D.; Maciá-Agulló, J.; Stucky, GD. (2014). Microwave synthesis of microstructured and nanostructured metal chalcogenides from elemental precursors in phosphonium ionic liquids. Journal of the American Chemical Society. 136(44):15465-15468. https://doi.org/10.1021/ja508628q es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://doi.org/10.1021/ja508628q es_ES
dc.description.upvformatpinicio 15465 es_ES
dc.description.upvformatpfin 15468 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 136 es_ES
dc.description.issue 44 es_ES
dc.relation.senia 286951 es_ES
dc.identifier.pmid 25333207
dc.contributor.funder National Science Foundation, EEUU
dc.contributor.funder U.S. Department of Energy


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