- -

Development of Coaxial Type flow microwave reactor

RiuNet: Institutional repository of the Polithecnic University of Valencia

Share/Send to

Cited by

Statistics

Development of Coaxial Type flow microwave reactor

Show simple item record

Files in this item

dc.contributor.author Matsumura, Takeko es_ES
dc.contributor.author Kishihara, M. es_ES
dc.contributor.author Urushihara, U. es_ES
dc.date.accessioned 2019-11-11T13:45:41Z
dc.date.available 2019-11-11T13:45:41Z
dc.date.issued 2019-10-15
dc.identifier.isbn 9788490487198
dc.identifier.uri http://hdl.handle.net/10251/130724
dc.description.abstract [EN] We have developed a flow microwave reactor with a coaxial cavity. It comprises a cylindrical cavity of 100 mm inside diameter, a metal rod along its center axis, and a spiral glass tube for flowing solvents and reactants, as shown in Fig.1. When the input port of microwave is placed at the end of the metal rod, the TEM mode is excited in the cylindrical chamber due to the presence of the metal rod. Simulations of the electric field and the magnetic field within the coaxial cavity are shown in Fig.2. This configuration was confirmed suitable for rapid and continuous microwave syntheses of various functional metal complexes. Experimental results are presented of Ir(Ⅲ) complexes for OLED dopants and Ru(Ⅱ) complexes for various sensors. The application to rapid and continuous microwave synthesis of various functional metal complexes were performed in success. In the similar manner as the coaxial reaction chamber of 2.45GHz, a coaxial reaction chamber for 5.8GHz IMS band, dimension of 51mm in diameter and 50mm in height, is designed The electric field distributions in the chamber and the temperature profiles of solvent are simulated using the commercial simulator (COMSOL Multiphysics) for 5.8 GHz, 5W microwave input. Using the simulation results appropriate dimensions of the chamber are determined for the 5.8 GHz operation. When water is used as a solvent the simulation shows that the temperature rises from20℃ to 95℃ after 300 seconds of the microwave irradiation. es_ES
dc.format.extent 5 es_ES
dc.language Inglés es_ES
dc.publisher Editorial Universitat Politècnica de València es_ES
dc.relation.ispartof AMPERE 2019. 17th International Conference on Microwave and High Frequency Heating es_ES
dc.rights Reconocimiento - No comercial - Sin obra derivada (by-nc-nd) es_ES
dc.subject Energy Production by Microwaves es_ES
dc.subject Microwave CVD es_ES
dc.subject EM Modelling es_ES
dc.subject Microwave Material interaction es_ES
dc.subject Dielectric Properties es_ES
dc.subject Dielectric Properties Measurement es_ES
dc.subject Solid State Microwave es_ES
dc.subject Microwave Processing es_ES
dc.subject Microwave Chemistry es_ES
dc.subject Microwave applicators design es_ES
dc.title Development of Coaxial Type flow microwave reactor es_ES
dc.type Capítulo de libro es_ES
dc.type Comunicación en congreso es_ES
dc.identifier.doi 10.4995/AMPERE2019.2019.9897
dc.rights.accessRights Abierto es_ES
dc.description.bibliographicCitation Matsumura, T.; Kishihara, M.; Urushihara, U. (2019). Development of Coaxial Type flow microwave reactor. En AMPERE 2019. 17th International Conference on Microwave and High Frequency Heating. Editorial Universitat Politècnica de València. 487-491. https://doi.org/10.4995/AMPERE2019.2019.9897 es_ES
dc.description.accrualMethod OCS es_ES
dc.relation.conferencename Ampere 2019 es_ES
dc.relation.conferencedate Septiembre 09-12,2019 es_ES
dc.relation.conferenceplace Valencia, Spain es_ES
dc.relation.publisherversion http://ocs.editorial.upv.es/index.php/AMPERE2019/AMPERE2019/paper/view/9897 es_ES
dc.description.upvformatpinicio 487 es_ES
dc.description.upvformatpfin 491 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.relation.pasarela OCS\9897 es_ES


This item appears in the following Collection(s)

Show simple item record