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Developing microwave chemistry under process engineering principles

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Developing microwave chemistry under process engineering principles

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dc.contributor.author Tioni, Estevan es_ES
dc.contributor.author Breysse, J. es_ES
dc.contributor.author Rousseaux, Pascal es_ES
dc.date.accessioned 2019-11-13T11:18:00Z
dc.date.available 2019-11-13T11:18:00Z
dc.date.issued 2019-10-15
dc.identifier.isbn 9788490487198
dc.identifier.uri http://hdl.handle.net/10251/130904
dc.description.abstract [EN] It is nowadays admitted that microwaves are frequently used in organic chemistry labs [1] (even if not as much as it was predicted 20 years ago, one must say [2]). On the other side it is also certain that this technology has not yet found its place in chemical industry: application at a production scale are very scarce [3][4] and this despite the potential advantages of the technology (selective heating, high heating rate, low thermal inertia…). The point is that mastering all the aspects of microwaves assisted synthesis at industrial scale demands a lot of different skills to work together: chemistry, process engineering, microwave engineering, materials science. This is so challenging that tools and methodologies for quantification of industrial microwave interest and scaling-up of lab results are missing. In this work we present our contributions to the deployment of microwaves for synthesis in the chemical industry which are mainly The development of small pilot reactors (1 L) in stainless steel, capable to withstand temperature and pressureThe application of a chemical engineering methodology to microwave assisted synthesisAn example of intensification (see table) of an industrially interesting reaction using microwave to access NPW (high temperature and pressure)A tentative of rationalization of process criteria to identify a priori the interest of microwave heating for a specific application [1]. Diaz-Ortiz et al., Chem. Rec. 2019, 19, 85–97 [2]. Kappe, Chem. Rec. 2019, 19, 15–39 [3]. Aldivia, brevet WO2004/066683A1 [4]. https://cen.acs.org/articles/94/i36/Microwaving-ton.html es_ES
dc.format.extent 7 es_ES
dc.language Inglés es_ES
dc.publisher Editorial Universitat Politècnica de València es_ES
dc.relation.ispartof AMPERE 2019. 17th International Conference on Microwave and High Frequency Heating es_ES
dc.rights Reconocimiento - No comercial - Sin obra derivada (by-nc-nd) es_ES
dc.subject Energy Production by Microwaves es_ES
dc.subject Microwave CVD es_ES
dc.subject EM Modelling es_ES
dc.subject Microwave Material interaction es_ES
dc.subject Dielectric Properties es_ES
dc.subject Dielectric Properties Measurement es_ES
dc.subject Solid State Microwave es_ES
dc.subject Microwave Processing es_ES
dc.subject Microwave Chemistry es_ES
dc.subject Microwave applicators design es_ES
dc.title Developing microwave chemistry under process engineering principles es_ES
dc.type Capítulo de libro es_ES
dc.type Comunicación en congreso es_ES
dc.identifier.doi 10.4995/AMPERE2019.2019.9901
dc.rights.accessRights Abierto es_ES
dc.description.bibliographicCitation Tioni, E.; Breysse, J.; Rousseaux, P. (2019). Developing microwave chemistry under process engineering principles. En AMPERE 2019. 17th International Conference on Microwave and High Frequency Heating. Editorial Universitat Politècnica de València. 174-180. https://doi.org/10.4995/AMPERE2019.2019.9901 es_ES
dc.description.accrualMethod OCS es_ES
dc.relation.conferencename Ampere 2019 es_ES
dc.relation.conferencedate Septiembre 09-12,2019 es_ES
dc.relation.conferenceplace Valencia, Spain es_ES
dc.relation.publisherversion http://ocs.editorial.upv.es/index.php/AMPERE2019/AMPERE2019/paper/view/9901 es_ES
dc.description.upvformatpinicio 174 es_ES
dc.description.upvformatpfin 180 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.relation.pasarela OCS\9901 es_ES


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