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Electrochemical fingerprint of archaeological lead silicate glasses from the voltammetry of microparticles approach

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Electrochemical fingerprint of archaeological lead silicate glasses from the voltammetry of microparticles approach

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dc.contributor.author Doménech Carbó, Antonio es_ES
dc.contributor.author Villegas Broncano, María Ángeles es_ES
dc.contributor.author Martínez Ramírez, Sagrario es_ES
dc.contributor.author Domenech Carbo, Mª Teresa es_ES
dc.contributor.author Martínez Pla, Betlem es_ES
dc.date.accessioned 2020-10-05T06:47:24Z
dc.date.available 2020-10-05T06:47:24Z
dc.date.issued 2016-12 es_ES
dc.identifier.issn 0002-7820 es_ES
dc.identifier.uri http://hdl.handle.net/10251/151089
dc.description.abstract [EN] The application of a solid-state electrochemical technique, voltammetry of microparticles (VMP), for studying archeological lead glass is described. Upon attachment to graphite electrodes immersed into aqueous acetate buffer, characteristic voltammetric profiles were obtained for submicrosamples of archeological glasses dated between the 9th and 19th centuries. Bivariate and multivariate chemometric analyses of the VMP data allowed us to characterize individual workshops/provenances which enabled a clear discrimination between soda-rich and potash-rich glasses. An analysis of the VMP data, combined by XRF, FESEM, AFM and ATR-FTIR and Micro-Raman spectroscopies, denoted the presence of Pb(IV) centers accompanying network-former and network-modifier Pb(II). es_ES
dc.description.sponsorship Financial support from the MINECO Projects CTQ2014-53736-C3-1-P, CTQ2014-53736-C3-2-P and MAT2015-65445-C2-2-R, which are supported with ERDF funds is gratefully acknowledged. Likewise financial support of the Comunidad de Madrid and structural funds of the EU through Programa Geomateriales 2 ref. S2013/MIT-2914 is acknowledged. The authors thank the Seccion de Investigacion Arqueologica Municipal de Valencia for kindly authorizing sampling to carry out this research. The authors also thank Dr. Jose Luis Moya Lopez and Mr. Manuel Planes Insausti (Microscopy Service of the Universitat Politecnica de Valencia) for their technical support. es_ES
dc.language Inglés es_ES
dc.publisher Blackwell Publishing es_ES
dc.relation.ispartof Journal of the American Ceramic Society es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Glass es_ES
dc.subject Archaeometry es_ES
dc.subject Voltammetry of microparticles es_ES
dc.subject FIB-FESEM-EDX es_ES
dc.subject Raman spectroscopy es_ES
dc.subject.classification PINTURA es_ES
dc.title Electrochemical fingerprint of archaeological lead silicate glasses from the voltammetry of microparticles approach es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1111/jace.14430 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//MAT2015-65445-C2-2-R/ES/RECUBRIMIENTOS MULTIFUNCIONALES MODIFICADOS CON AGENTES DE RETROALIMENTACION ACTIVA PARA LA PROTECCION DE MATERIALES Y COLECCIONES DEL PATRIMONIO CULTURAL/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/CAM//S2013%2FMIT-2914/ES/Tecnologías y conservación de geomateriales del patrimonio/GEOMETARIALES2-CM/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//CTQ2014-53736-C3-1-P/ES/APLICACION DE LAS TECNICAS NANOELECTROQUIMICAS Y BIOTECNOLOGIAS EN EL ESTUDIO Y CONSERVACION DEL PATRIMONIO EN METAL/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Conservación y Restauración de Bienes Culturales - Departament de Conservació i Restauració de Béns Culturals es_ES
dc.description.bibliographicCitation Doménech Carbó, A.; Villegas Broncano, MÁ.; Martínez Ramírez, S.; Domenech Carbo, MT.; Martínez Pla, B. (2016). Electrochemical fingerprint of archaeological lead silicate glasses from the voltammetry of microparticles approach. Journal of the American Ceramic Society. 99(12):3915-3923. https://doi.org/10.1111/jace.14430 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://doi.org/10.1111/jace.14430 es_ES
dc.description.upvformatpinicio 3915 es_ES
dc.description.upvformatpfin 3923 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 99 es_ES
dc.description.issue 12 es_ES
dc.relation.pasarela S\326845 es_ES
dc.contributor.funder European Commission es_ES
dc.contributor.funder Instituto de Salud Carlos III es_ES
dc.contributor.funder European Regional Development Fund es_ES
dc.contributor.funder Ministerio de Economía y Competitividad es_ES
dc.contributor.funder Comunidad de Madrid
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