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Photoelectrochemical removal of chlorfenvinphos by using WO3 nanorods: Influence of annealing temperature and operation pH

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Photoelectrochemical removal of chlorfenvinphos by using WO3 nanorods: Influence of annealing temperature and operation pH

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dc.contributor.author Fernández Domene, Ramón Manuel es_ES
dc.contributor.author Roselló-Márquez, Gemma es_ES
dc.contributor.author Sánchez Tovar, Rita es_ES
dc.contributor.author Lucas-Granados, Bianca es_ES
dc.contributor.author Garcia-Anton, Jose es_ES
dc.date.accessioned 2021-01-21T04:32:19Z
dc.date.available 2021-01-21T04:32:19Z
dc.date.issued 2019-04-01 es_ES
dc.identifier.issn 1383-5866 es_ES
dc.identifier.uri http://hdl.handle.net/10251/159615
dc.description.abstract [EN] A visible-light driven photoelectrochemical degradation process has been applied to a solution polluted with the organophosphate insecticide chlorfenvinphos. Different WO3 nanosheets/nanorods have been used as photoanodes. These nanostructured electrodes have been fabricated by anodization of tungsten and, subsequently, they have been subjected to a thermal treatment (annealing). The combined influence of annealing temperature (400¿°C and 600¿°C) and operation pH (1 and 3) on the photoelectrocatalytic behavior of these nanorods has been examined through a statistical analysis. Morphological, structural and photoelectrochemical characterizations have also been carried out. The chlorfenvinphos degradation efficiency depended both on annealing temperature and, specially, operation pH. At pH 1 and using an annealing temperature of 600¿°C, chlorfenvinphos has been effectively degraded following pseudo-first order kinetics with a coefficient of 7.8¿×¿10¿3¿min¿1, and notably mineralized (more than 65% of Total Organic Carbon decrease). es_ES
dc.description.sponsorship Authors thank for the financial support to the Ministerio de Economia y Competitividad (Project Code: CTQ2016-79203-R), for its help in the Laser Raman Microscope acquisition (UPOV08-3E-012) and for the co-finance by the European Social Fund. Ramon M. Fernandez Domene thanks the UPV for the concession of a post-doctoral grant (PAID-10-17) and Gemma Rosello Marquez also thanks the Generalitat Valenciana for the concession of a pre-doctoral grant (ACIF/2018/159) es_ES
dc.language Inglés es_ES
dc.publisher Elsevier es_ES
dc.relation.ispartof Separation and Purification Technology es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Photoelectrochemical degradation es_ES
dc.subject WO3 nanorods es_ES
dc.subject Anodization es_ES
dc.subject Chlorfenvinphos es_ES
dc.subject Regression model es_ES
dc.subject.classification INGENIERIA QUIMICA es_ES
dc.title Photoelectrochemical removal of chlorfenvinphos by using WO3 nanorods: Influence of annealing temperature and operation pH es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1016/j.seppur.2018.11.049 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MEC//UPOV08-3E-001/ES/Utilización de Desktop Microscopy System (DMS) en el campo de los materiales/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/UPV//PAID-10-17/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//CTQ2016-79203-R/ES/MODIFICACION DE FOTOCATALIZADORES DE OXIDOS METALICOS NANOESTRUCTURADOS PARA LA ELIMINACION DE FARMACOS Y PRODUCCION ENERGETICA/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/GVA//ACIF%2F2018%2F159/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Ingeniería Química y Nuclear - Departament d'Enginyeria Química i Nuclear es_ES
dc.description.bibliographicCitation Fernández Domene, RM.; Roselló-Márquez, G.; Sánchez Tovar, R.; Lucas-Granados, B.; Garcia-Anton, J. (2019). Photoelectrochemical removal of chlorfenvinphos by using WO3 nanorods: Influence of annealing temperature and operation pH. Separation and Purification Technology. 212:458-464. https://doi.org/10.1016/j.seppur.2018.11.049 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.1016/j.seppur.2018.11.049 es_ES
dc.description.upvformatpinicio 458 es_ES
dc.description.upvformatpfin 464 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 212 es_ES
dc.relation.pasarela S\377124 es_ES
dc.contributor.funder European Social Fund es_ES
dc.contributor.funder Generalitat Valenciana es_ES
dc.contributor.funder Universitat Politècnica de València es_ES
dc.contributor.funder Ministerio de Economía y Competitividad es_ES
dc.contributor.funder Ministerio de Educación y Ciencia es_ES
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