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Development of multilayer Hydroxyapatite - Ag/TiN-Ti coatings deposited by radio frequency magnetron sputtering with potential application in the biomedical field

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Development of multilayer Hydroxyapatite - Ag/TiN-Ti coatings deposited by radio frequency magnetron sputtering with potential application in the biomedical field

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dc.contributor.author Lenis, J.A. es_ES
dc.contributor.author Bejarano, G. es_ES
dc.contributor.author Rico Tortosa, Patricia María es_ES
dc.contributor.author Gómez Ribelles, José Luís es_ES
dc.contributor.author Bolívar, F.J. es_ES
dc.date.accessioned 2021-02-02T04:33:00Z
dc.date.available 2021-02-02T04:33:00Z
dc.date.issued 2019-11-15 es_ES
dc.identifier.issn 0257-8972 es_ES
dc.identifier.uri http://hdl.handle.net/10251/160436
dc.description "NOTICE: this is the author's version of a work that was accepted for publication in Surface and Coatings Technology. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Surface and Coatings Technology, VOL 377, (2019) DOI 10.1016/j.surfcoat.2019.06.097" es_ES
dc.description.abstract [EN] The use of composite coatings is emerging as a great alternative to conventional coatings, allowing the combination of different superficial properties that are widely desired in surgical implants, such as osteointegration and bactericidal character, and cannot be provided by one material alone. In the present investigation the effect of the incorporation of a TiN-Ti intermediate bilayer on the chemical composition, structure, morphology, roughness, residual stresses and adhesion of a multi-layer Hydroxyapatite (HA)-Ag coating deposited on Ti-6Al-4V by magnetron sputtering was evaluated. Additionally, the cytotoxicity of the developed system was evaluated by in vitro tests. According to the results obtained, a decrease in the Ca/P ratio from 1.85 to 1.74 was obtained through the deposition of an HA-Ag system on the intermediate bilayer, and the crystallinity of the developed coating was favored. The multi-layer structure was effectively observed by field emission scanning electron microscopy, where it was possible to identify each of the HA, Ag, TiN and Ti layers. Meanwhile, an increase of 7% in crystallite size, a decrease of 36% in residual stresses and an increase of 32% in adhesion were registered for this composite coating compared to the free intermediate bilayer system. Finally, biological evaluation allowed the non-cytotoxic character of the deposited coatings to be confirmed. es_ES
dc.description.sponsorship We thank the University of Antioquia, the Centro de Investigation, Innovation y Desarrollo de materiales (CIDEMAT) group, the Departamento Administrativo de Ciencia, Tecnologia e Innovation (COLCIENCIAS) for financing the Project 15-1696, the scholarship program of Enlazamundos, PR and JLGR acknowledge financial support from the Spanish Ministry of Economy and Competitiveness (MINECO) through the project MAT2016-76039-C4-1-R (AEI/FEDER, UE) (including the FEDER financial support). CIBER-BBN is an initiative funded by the VI National R&D&I Plan 2008-2011, Iniciativa Ingenio 2010, Consolider Program. CIBER Actions are financed by the Institute de Salud Carlos III with assistance from the European Regional Development Fund. es_ES
dc.language Inglés es_ES
dc.publisher Elsevier es_ES
dc.relation.ispartof Surface and Coatings Technology es_ES
dc.rights Reconocimiento - No comercial - Sin obra derivada (by-nc-nd) es_ES
dc.subject Magnetron sputtering es_ES
dc.subject Hydroxyapatite es_ES
dc.subject Calcium/phosphate ratio es_ES
dc.subject Microstructure es_ES
dc.subject Multi-layer coating es_ES
dc.subject Intermediate layers es_ES
dc.subject Critical load es_ES
dc.subject Cytotoxicity es_ES
dc.subject.classification MAQUINAS Y MOTORES TERMICOS es_ES
dc.title Development of multilayer Hydroxyapatite - Ag/TiN-Ti coatings deposited by radio frequency magnetron sputtering with potential application in the biomedical field es_ES
dc.type Artículo es_ES
dc.type Comunicación en congreso es_ES
dc.identifier.doi 10.1016/j.surfcoat.2019.06.097 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//MAT2016-76039-C4-1-R/ES/BIOMATERIALES PIEZOELECTRICOS PARA LA DIFERENCIACION CELULAR EN INTERFASES CELULA-MATERIAL ELECTRICAMENTE ACTIVAS/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/COLCIENCIAS//15-1696/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Termodinámica Aplicada - Departament de Termodinàmica Aplicada es_ES
dc.contributor.affiliation Universitat Politècnica de València. Centro de Biomateriales e Ingeniería Tisular - Centre de Biomaterials i Enginyeria Tissular es_ES
dc.description.bibliographicCitation Lenis, J.; Bejarano, G.; Rico Tortosa, PM.; Gómez Ribelles, JL.; Bolívar, F. (2019). Development of multilayer Hydroxyapatite - Ag/TiN-Ti coatings deposited by radio frequency magnetron sputtering with potential application in the biomedical field. Surface and Coatings Technology. 377:1-9. https://doi.org/10.1016/j.surfcoat.2019.06.097 es_ES
dc.description.accrualMethod S es_ES
dc.relation.conferencename International Conference on Metallurgical Coatings and Thin Films (ICMCTF 2019) es_ES
dc.relation.conferencedate Mayo 19-24,2019 es_ES
dc.relation.conferenceplace San Diego, CA, USA es_ES
dc.relation.publisherversion https://doi.org/10.1016/j.surfcoat.2019.06.097 es_ES
dc.description.upvformatpinicio 1 es_ES
dc.description.upvformatpfin 9 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 377 es_ES
dc.relation.pasarela S\405041 es_ES
dc.contributor.funder Universidad de Antioquia es_ES
dc.contributor.funder Instituto de Salud Carlos III es_ES
dc.contributor.funder European Regional Development Fund es_ES
dc.contributor.funder Ministerio de Ciencia e Innovación es_ES
dc.contributor.funder Ministerio de Economía y Competitividad es_ES
dc.contributor.funder Departamento Administrativo de Ciencia, Tecnología e Innovación, Colombia es_ES
dc.contributor.funder Centro de Investigación Biomédica en Red en Bioingeniería, Biomateriales y Nanomedicina es_ES
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dc.subject.ods 03.- Garantizar una vida saludable y promover el bienestar para todos y todas en todas las edades es_ES


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