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Production strategies of asymmetric BaCe0.65Zr0.20Y0.15O3-delta - Ce(0.8)Gd(0.2)O(2-delta) membrane for hydrogen separation

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Production strategies of asymmetric BaCe0.65Zr0.20Y0.15O3-delta - Ce(0.8)Gd(0.2)O(2-delta) membrane for hydrogen separation

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dc.contributor.author Mercadelli, Elisa es_ES
dc.contributor.author Gondolini, Angela es_ES
dc.contributor.author Montaleone, Daniel es_ES
dc.contributor.author Pinasco, Paola es_ES
dc.contributor.author Escolástico Rozalén, Sonia es_ES
dc.contributor.author Serra Alfaro, José Manuel es_ES
dc.contributor.author Sanson, Alessandra es_ES
dc.date.accessioned 2021-02-10T04:31:37Z
dc.date.available 2021-02-10T04:31:37Z
dc.date.issued 2020-03-04 es_ES
dc.identifier.issn 0360-3199 es_ES
dc.identifier.uri http://hdl.handle.net/10251/160984
dc.description.abstract [EN] Mixed proton and electron conductor ceramic composites are among the most promising materials for hydrogen separation membrane technology especially if designed in an asymmetrical configuration (thin membrane supported onto a thicker porous substrate). However a precise processing optimization is needed to effectively obtain planar and crack free asymmetrical membranes with suitable microstructure and composition without affecting their hydrogen separation efficiency. This work highlights for the first time the most critical issues linked to the tape casting process used to obtain BaCe0.65Zr0.20Y0.15O3-delta - Ce0.8Gd0.2O2-delta (BCZY-GDC) asymmetrical membranes for H-2 separation. The critical role of the co-firing process, sintering aid and atmosphere was critically investigated. The optimization of the production strategy allowed to obtain asymmetric membranes constituted by a dense 20 mu m-thick ceramic-ceramic composite layer supported by a porous (36%) 750 mu m-thick BCZY-GDC substrate. The asymmetric membranes here reported showed H2 fluxes (0.47 mL min(-1) cm(-2) at 750 degrees C) among the highest obtained for an all-ceramic membrane. es_ES
dc.description.sponsorship This work has been funded by the agreement between the Italian Ministry of Economic Development and the Italian National Research Council "Ricerca di sistema elettrico nazionale" es_ES
dc.language Inglés es_ES
dc.publisher Elsevier es_ES
dc.relation.ispartof International Journal of Hydrogen Energy es_ES
dc.rights Reconocimiento - No comercial - Sin obra derivada (by-nc-nd) es_ES
dc.subject Tape casting es_ES
dc.subject BCZY-GDC es_ES
dc.subject Ceramic membranes es_ES
dc.subject Microstructure es_ES
dc.title Production strategies of asymmetric BaCe0.65Zr0.20Y0.15O3-delta - Ce(0.8)Gd(0.2)O(2-delta) membrane for hydrogen separation es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1016/j.ijhydene.2019.03.148 es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Instituto Universitario Mixto de Tecnología Química - Institut Universitari Mixt de Tecnologia Química es_ES
dc.description.bibliographicCitation Mercadelli, E.; Gondolini, A.; Montaleone, D.; Pinasco, P.; Escolástico Rozalén, S.; Serra Alfaro, JM.; Sanson, A. (2020). Production strategies of asymmetric BaCe0.65Zr0.20Y0.15O3-delta - Ce(0.8)Gd(0.2)O(2-delta) membrane for hydrogen separation. International Journal of Hydrogen Energy. 45(12):7468-7478. https://doi.org/10.1016/j.ijhydene.2019.03.148 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.1016/j.ijhydene.2019.03.148 es_ES
dc.description.upvformatpinicio 7468 es_ES
dc.description.upvformatpfin 7478 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 45 es_ES
dc.description.issue 12 es_ES
dc.relation.pasarela S\417947 es_ES
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