- -

Evidence of a new phase in gypsum-anhydrite transformations under microwave heating by in situ dielectric analysis and Raman spectroscopy

RiuNet: Institutional repository of the Polithecnic University of Valencia

Share/Send to

Cited by

Statistics

Evidence of a new phase in gypsum-anhydrite transformations under microwave heating by in situ dielectric analysis and Raman spectroscopy

Show full item record

López-Buendía, AM.; García-Baños, B.; Urquiola, MM.; Catalá Civera, JM.; Penaranda-Foix, FL. (2020). Evidence of a new phase in gypsum-anhydrite transformations under microwave heating by in situ dielectric analysis and Raman spectroscopy. Physical Chemistry Chemical Physics. 22(47):27713-27723. https://doi.org/10.1039/d0cp04926c

Por favor, use este identificador para citar o enlazar este ítem: http://hdl.handle.net/10251/166839

Files in this item

Item Metadata

Title: Evidence of a new phase in gypsum-anhydrite transformations under microwave heating by in situ dielectric analysis and Raman spectroscopy
Author: López-Buendía, Angel M. García-Baños, Beatriz Urquiola, M. Mar Catalá Civera, José Manuel Penaranda-Foix, Felipe L.
UPV Unit: Universitat Politècnica de València. Departamento de Comunicaciones - Departament de Comunicacions
Issued date:
Abstract:
[EN] Mineral transformations of the gypsum-anhydrite system under microwave heating have been studied using in situ dielectric thermal analysis (MW-DETA) and Raman spectroscopy simultaneously. The dielectric properties of ...[+]
Copyrigths: Reconocimiento - No comercial (by-nc)
Source:
Physical Chemistry Chemical Physics. (issn: 1463-9076 )
DOI: 10.1039/d0cp04926c
Publisher:
The Royal Society of Chemistry
Publisher version: https://doi.org/10.1039/d0cp04926c
Type: Artículo

References

A. C. Metaxas and R. J.Meredith , Industrial microwave heating , Peregrinus , London , 1983

Mishra, R. R., & Sharma, A. K. (2016). Microwave–material interaction phenomena: Heating mechanisms, challenges and opportunities in material processing. Composites Part A: Applied Science and Manufacturing, 81, 78-97. doi:10.1016/j.compositesa.2015.10.035

Gutiérrez, J. D., Catalá-Civera, J. M., Bows, J., & Peñaranda-Foix, F. L. (2017). Dynamic measurement of dielectric properties of food snack pellets during microwave expansion. Journal of Food Engineering, 202, 1-8. doi:10.1016/j.jfoodeng.2017.01.021 [+]
A. C. Metaxas and R. J.Meredith , Industrial microwave heating , Peregrinus , London , 1983

Mishra, R. R., & Sharma, A. K. (2016). Microwave–material interaction phenomena: Heating mechanisms, challenges and opportunities in material processing. Composites Part A: Applied Science and Manufacturing, 81, 78-97. doi:10.1016/j.compositesa.2015.10.035

Gutiérrez, J. D., Catalá-Civera, J. M., Bows, J., & Peñaranda-Foix, F. L. (2017). Dynamic measurement of dielectric properties of food snack pellets during microwave expansion. Journal of Food Engineering, 202, 1-8. doi:10.1016/j.jfoodeng.2017.01.021

Kingman, S. W., & Rowson, N. A. (1998). Microwave treatment of minerals-a review. Minerals Engineering, 11(11), 1081-1087. doi:10.1016/s0892-6875(98)00094-6

Kingman, S. W. (2006). Recent developments in microwave processing of minerals. International Materials Reviews, 51(1), 1-12. doi:10.1179/174328006x79472

Lovás, M., Kováčová, M., Dimitrakis, G., Čuvanová, S., Znamenáčková, I., & Jakabský, Š. (2010). Modeling of microwave heating of andesite and minerals. International Journal of Heat and Mass Transfer, 53(17-18), 3387-3393. doi:10.1016/j.ijheatmasstransfer.2010.03.012

S. M. J. Koleini and K.Barani in The development and application of microwave heating , ed. Wenbin C. , IntechOpen , London , 2012 , ch. 4, p. 79

A. M. López-Buendía , B.García-Baños , J.Bastida , G.Llorens-Vallés , M. M.Urquiola and J. M.Catalá-Civera , presented at 3GCMEA, Cartagena, Spain, July 2016

Reinosa, J. J., García-Baños, B., Catalá-Civera, J. M., & Fernández, J. F. (2019). A step ahead on efficient microwave heating for kaolinite. Applied Clay Science, 168, 237-243. doi:10.1016/j.clay.2018.11.001

Kitchen, H. J., Vallance, S. R., Kennedy, J. L., Tapia-Ruiz, N., Carassiti, L., Harrison, A., … Gregory, D. H. (2013). Modern Microwave Methods in Solid-State Inorganic Materials Chemistry: From Fundamentals to Manufacturing. Chemical Reviews, 114(2), 1170-1206. doi:10.1021/cr4002353

Sun, J., Wang, W., & Yue, Q. (2016). Review on Microwave-Matter Interaction Fundamentals and Efficient Microwave-Associated Heating Strategies. Materials, 9(4), 231. doi:10.3390/ma9040231

Wu, L., Zhang, Y., Wang, F., Ma, W., Xie, T., & Huang, K. (2019). An On-Line System for High Temperature Dielectric Property Measurement of Microwave-Assisted Sintering Materials. Materials, 12(4), 665. doi:10.3390/ma12040665

R. N. Clarke , A. P.Gregory , D.Cannell , M.Patrick , S.Wylie , I.Youngs and G.Hill , Technical Report, Institute of Measurement and Control/National Physical Laboratory, 2003

Garcia-Baños, B., Catalá-Civera, J., Peñaranda-Foix, F., Plaza-González, P., & Llorens-Vallés, G. (2016). In Situ Monitoring of Microwave Processing of Materials at High Temperatures through Dielectric Properties Measurement. Materials, 9(5), 349. doi:10.3390/ma9050349

García-Baños, B., Catalá-Civera, J. M., Sánchez, J. R., Navarrete, L., López-Buendía, A. M., & Schmidt, L. (2020). High Temperature Dielectric Properties of Iron- and Zinc-Bearing Products during Carbothermic Reduction by Microwave Heating. Metals, 10(5), 693. doi:10.3390/met10050693

Catala-Civera, J. M., Canos, A. J., Plaza-Gonzalez, P., Gutierrez, J. D., Garcia-Banos, B., & Penaranda-Foix, F. L. (2015). Dynamic Measurement of Dielectric Properties of Materials at High Temperature During Microwave Heating in a Dual Mode Cylindrical Cavity. IEEE Transactions on Microwave Theory and Techniques, 63(9), 2905-2914. doi:10.1109/tmtt.2015.2453263

Hildyard, R. C., Llana-Funez, S., Wheeler, J., Faulkner, D. R., & Prior, D. J. (2011). Electron Backscatter Diffraction (EBSD) Analysis of Bassanite Transformation Textures and Crystal Structure Produced from Experimentally Deformed and Dehydrated Gypsum. Journal of Petrology, 52(5), 839-856. doi:10.1093/petrology/egr004

Azam, S. (2006). Study on the geological and engineering aspects of anhydrite/gypsum transition in the Arabian Gulf coastal deposits. Bulletin of Engineering Geology and the Environment, 66(2), 177-185. doi:10.1007/s10064-006-0053-2

Tesárek, P., Drchalová, J., Kolísko, J., Rovnaníková, P., & Černý, R. (2007). Flue gas desulfurization gypsum: Study of basic mechanical, hydric and thermal properties. Construction and Building Materials, 21(7), 1500-1509. doi:10.1016/j.conbuildmat.2006.05.009

Singh, M., & Garg, M. (2000). Making of anhydrite cement from waste gypsum. Cement and Concrete Research, 30(4), 571-577. doi:10.1016/s0008-8846(00)00209-x

Charola, A. E., Pühringer, J., & Steiger, M. (2006). Gypsum: a review of its role in the deterioration of building materials. Environmental Geology, 52(2), 339-352. doi:10.1007/s00254-006-0566-9

K. K. Kelley , C. T.Anderson and J. C.Southartd , USD Interior Tech, Paper 625

Valimbe, P. (2002). Effects of water content and temperature on the crystallization behavior of FGD scrubber sludge. Fuel, 81(10), 1297-1304. doi:10.1016/s0016-2361(02)00045-5

James, A. N., & Lupton, A. R. R. (1978). Gypsum and anhydrite in foundations of hydraulic structures. Géotechnique, 28(3), 249-272. doi:10.1680/geot.1978.28.3.249

Ko, S., Olgaard, D. L., & Briegel, U. (1995). The transition from weakening to strengthening in dehydrating gypsum: Evolution of excess pore pressures. Geophysical Research Letters, 22(9), 1009-1012. doi:10.1029/95gl00886

Anonymous Mineral Commodity Summaries 2019, Reston, VA, 2019

W. Chun , S.Kim and K.Lee , ‘EuroDrying2011’, 2011

Kasparaitė, D., Lukošenkinaitė, L., Valančius, Z., Kybartienė, N., & Leškevičienė, V. (2013). Microwave use of gypsum dehydration feasibility study. Chemical Technology, 63(1). doi:10.5755/j01.ct.63.1.4518

Boeyens, J. C. A., & Ichharam, V. V. H. (2002). Redetermination of the crystal structure of calcium sulphate dihydrate, CaSO4 · 2H2O. Zeitschrift für Kristallographie - New Crystal Structures, 217(JG), 9-10. doi:10.1524/ncrs.2002.217.jg.9

Schofield, P. F., Knight, K. S., & Stretton, I. C. (1996). Thermal expansion of gypsum investigated by neutron powder diffraction. American Mineralogist, 81(7-8), 847-851. doi:10.2138/am-1996-7-807

Schmidt, H., Paschke, I., Freyer, D., & Voigt, W. (2011). Water channel structure of bassanite at high air humidity: crystal structure of CaSO4·0.625H2O. Acta Crystallographica Section B Structural Science, 67(6), 467-475. doi:10.1107/s0108768111041759

Bezou, C., Nonat, A., Mutin, J.-C., Christensen, A. N., & Lehmann, M. S. (1995). Investigation of the Crystal Structure of γ-CaSO4, CaSO4 · 0.5 H2O, and CaSO4 · 0.6 H2O by Powder Diffraction Methods. Journal of Solid State Chemistry, 117(1), 165-176. doi:10.1006/jssc.1995.1260

Christensen, A. N., Olesen, M., Cerenius, Y., & Jensen, T. R. (2008). Formation and Transformation of Five Different Phases in the CaSO4−H2O System: Crystal Structure of the Subhydrate β-CaSO4·0.5H2O and Soluble Anhydrite CaSO4. Chemistry of Materials, 20(6), 2124-2132. doi:10.1021/cm7027542

Follner, S., Wolter, A., Preusser, A., Indris, S., Silber, C., & Follner, H. (2002). The Setting Behaviour of α- and β-CaSO4 · 0,5 H2O as a Function of Crystal Structure and Morphology. Crystal Research and Technology, 37(10), 1075-1087. doi:10.1002/1521-4079(200210)37:10<1075::aid-crat1075>3.0.co;2-x

MORRIS, R. J. (1963). X-ray Diffraction Identification of the Alpha- and Beta-forms of Calcium Sulphate Hemihydrate. Nature, 198(4887), 1298-1299. doi:10.1038/1981298a0

Vellmer, C., Middendorf, B., & Singh, N. B. (2006). Hydration of α-hemihydrate in the presence of carboxylic acids. Journal of Thermal Analysis and Calorimetry, 86(3), 721-726. doi:10.1007/s10973-005-7224-4

Prieto-Taboada, N., Larrañaga, A., Gómez-Laserna, O., Martínez-Arkarazo, I., Olazabal, M. A., & Madariaga, J. M. (2015). The relevance of the combination of XRD and Raman spectroscopy for the characterization of the CaSO4–H2O system compounds. Microchemical Journal, 122, 102-109. doi:10.1016/j.microc.2015.04.010

Sipple, E.-M., Bracconi, P., Dufour, P., & Mutin, J.-C. (2001). Microstructural modifications resulting from the dehydration of gypsum. Solid State Ionics, 141-142, 447-454. doi:10.1016/s0167-2738(01)00755-x

Carbone, M., Ballirano, P., & Caminiti, R. (2008). Kinetics of gypsum dehydration at reduced pressure: an energy dispersive X-ray diffraction study. European Journal of Mineralogy, 20(4), 621-627. doi:10.1127/0935-1221/2008/0020-1826

A. M. López-Buendía , C.Suesta , J. M.Cuevas , M. M.Urquiola and J.Bastida , presented at 12th EMABM, 2009, 443

Zhao, Z. M., Wang, C. J., Li, C. Q., & Zhang, X. M. (2013). On Experimental Study of Development Calcined Gypsum from Flue Gas Desulfurization by Microwave Technology. Applied Mechanics and Materials, 368-370, 780-784. doi:10.4028/www.scientific.net/amm.368-370.780

Kirfel, A., & Will, G. (1980). Charge density in anhydrite, CaSO4, from X-ray and neutron diffraction measurements. Acta Crystallographica Section B Structural Crystallography and Crystal Chemistry, 36(12), 2881-2890. doi:10.1107/s0567740880010461

Gracia, L., Beltrán, A., Errandonea, D., & Andrés, J. (2011). CaSO4 and Its Pressure-Induced Phase Transitions. A Density Functional Theory Study. Inorganic Chemistry, 51(3), 1751-1759. doi:10.1021/ic202056b

Crichton, W. A., Parise, J. B., Antao, S. M., & Grzechnik, A. (2005). Evidence for monazite-, barite-, and AgMnO4(distorted barite)-type structures of CaSO4at high pressure and temperature. American Mineralogist, 90(1), 22-27. doi:10.2138/am.2005.1654

Pedersen, B. F., & Semmingsen, D. (1982). Neutron diffraction refinement of the structure of gypsum, CaSO4.2H2O. Acta Crystallographica Section B Structural Crystallography and Crystal Chemistry, 38(4), 1074-1077. doi:10.1107/s0567740882004993

De la Torre, Á. G., López-Olmo, M.-G., Álvarez-Rua, C., García-Granda, S., & Aranda, M. A. G. (2004). Structure and microstructure of gypsum and its relevance to Rietveld quantitative phase analyses. Powder Diffraction, 19(3), 240-246. doi:10.1154/1.1725254

Hartman, P. (1989). On the unit cell dimensions and bond lengths of anhydrite. European Journal of Mineralogy, 1(5), 721-722. doi:10.1127/ejm/1/5/0721

Morikawa, H., Minato, I., Tomita, T., & Iwai, S. (1975). Anhydrite: a refinement. Acta Crystallographica Section B Structural Crystallography and Crystal Chemistry, 31(8), 2164-2165. doi:10.1107/s0567740875007145

Prieto-Taboada, N., Gómez-Laserna, O., Martínez-Arkarazo, I., Olazabal, M. Á., & Madariaga, J. M. (2014). Raman Spectra of the Different Phases in the CaSO4–H2O System. Analytical Chemistry, 86(20), 10131-10137. doi:10.1021/ac501932f

Antao, S. M. (2011). Crystal-structure analysis of four mineral samples of anhydrite, CaSO4, using synchrotron high-resolution powder X-ray diffraction data. Powder Diffraction, 26(4), 326-330. doi:10.1154/1.3659285

Borg, I. Y., & Smith, D. K. (1975). A high pressure polymorph of CaSO4. Contributions to Mineralogy and Petrology, 50(2), 127-133. doi:10.1007/bf00373332

Mukhopadhyay, A., Cole, W. T. S., & Saykally, R. J. (2015). The water dimer I: Experimental characterization. Chemical Physics Letters, 633, 13-26. doi:10.1016/j.cplett.2015.04.016

Kaatze, U. (1989). Complex permittivity of water as a function of frequency and temperature. Journal of Chemical & Engineering Data, 34(4), 371-374. doi:10.1021/je00058a001

Ellison, W. J. (2007). Permittivity of Pure Water, at Standard Atmospheric Pressure, over the Frequency Range 0–25THz and the Temperature Range 0–100°C. Journal of Physical and Chemical Reference Data, 36(1), 1-18. doi:10.1063/1.2360986

García-Baños, B., Reinosa, J. J., Peñaranda-Foix, F. L., Fernández, J. F., & Catalá-Civera, J. M. (2019). Temperature Assessment Of Microwave-Enhanced Heating Processes. Scientific Reports, 9(1). doi:10.1038/s41598-019-47296-0

Gutierrez-Cano, J. D., Plaza-Gonzalez, P., Canos, A. J., Garcia-Banos, B., Catala-Civera, J. M., & Penaranda-Foix, F. L. (2020). A New Stand-Alone Microwave Instrument for Measuring the Complex Permittivity of Materials at Microwave Frequencies. IEEE Transactions on Instrumentation and Measurement, 69(6), 3595-3605. doi:10.1109/tim.2019.2941038

Berenblut, B. J., Dawson, P., & Wilkinson, G. R. (1973). A comparison of the Raman spectra of anhydrite (CaSO4) and gypsum (CaSO4).2H2O). Spectrochimica Acta Part A: Molecular Spectroscopy, 29(1), 29-36. doi:10.1016/0584-8539(73)80005-4

Simon, B., & Bienfait, M. (1965). Structure et mécanisme de croissance du gypse. Acta Crystallographica, 19(5), 750-756. doi:10.1107/s0365110x65004310

Massaro, F. R., Rubbo, M., & Aquilano, D. (2010). Theoretical Equilibrium Morphology of Gypsum (CaSO4·2H2O). 1. A Syncretic Strategy to Calculate the Morphology of Crystals. Crystal Growth & Design, 10(7), 2870-2878. doi:10.1021/cg900660v

Khasanov, R. A., Nizamutdinov, N. M., Khasanova, N. M., Gubaĭdullin, A. T., & Vinokurov, V. M. (2008). Low-temperature dehydration of gypsum single crystals. Crystallography Reports, 53(5), 806-811. doi:10.1134/s1063774508050143

W. Smykatz-Kloss , K.Heide and W.Klinke in Handbook of Thermal Analysis and Calorimetry , ed. M. E. Brown and P. K. Gallagher , Elsevier , 2003 , ch. 11, vol. 2, p. 451

Carvalho, M. T. M., Leles, M. I. G., & Tubino, R. M. C. (2008). TG and DSC studies on plaster residues as recycled material. Journal of Thermal Analysis and Calorimetry, 91(2), 621-625. doi:10.1007/s10973-006-8169-y

B. Gacía-Baños , A. M.López-Buendía , C.Suesta , J. M.Catalá-Civera ., J.Jiménez Reinosa and J. F.Fernández , 15th International Conference on Microwave and High Frequency Heating , 2015, Krakow (Poland), p. 107

Alford, N. M., Breeze, J., Wang, X., Penn, S. J., Dalla, S., Webb, S. J., … Aupi, X. (2001). Dielectric loss of oxide single crystals and polycrystalline analogues from 10 to 320 K. Journal of the European Ceramic Society, 21(15), 2605-2611. doi:10.1016/s0955-2219(01)00324-7

Baker-Jarvis, J., & Kim, S. (2012). The Interaction of Radio-Frequency Fields with Dielectric Materials at Macroscopic to Mesoscopic Scales. Journal of Research of the National Institute of Standards and Technology, 117, 1. doi:10.6028/jres.117.001

[-]

recommendations

 

This item appears in the following Collection(s)

Show full item record