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Determination of the optimum parameters in the high resolution thermogravimetric analysis (HRTG) for cementitious materials

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Determination of the optimum parameters in the high resolution thermogravimetric analysis (HRTG) for cementitious materials

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dc.contributor.author Ivan Tobón, Jorge es_ES
dc.contributor.author Paya Bernabeu, Jorge Juan es_ES
dc.contributor.author Borrachero Rosado, María Victoria es_ES
dc.contributor.author Soriano Martínez, Lourdes es_ES
dc.contributor.author Restrepo Baena, Oscar Jaime es_ES
dc.date.accessioned 2015-04-21T09:10:13Z
dc.date.available 2015-04-21T09:10:13Z
dc.date.issued 2012
dc.identifier.issn 1388-6150
dc.identifier.uri http://hdl.handle.net/10251/49040
dc.description.abstract In this article, the methodology to implementation of high resolution thermogravimetric analysis (HRTG) for construction materials like Portland cement pastes is presented. The aim of this technique is to make easier the identification of the decomposition reactions that frequently are overlapping on conventional thermogravimetric analysis (TG) like is the case of some mineral phases in the cement pastes. The optimum parameters related to sample mass and purge flow gas were established. It is necessary carried out the analysis with high quantity of sample (60 mg in this case) and without purge gas in order to get better results and excellent reproducibility. The tests have average heating rate higher than 3 °C min -1 in the temperature range studied (35-300 °C), showing that the HRTG is not time-expensive technique. © 2010 Akadémiai Kiadó, Budapest, Hungary. es_ES
dc.language Inglés es_ES
dc.publisher Akadémiai Kiadó es_ES
dc.relation.ispartof Journal of Thermal Analysis and Calorimetry es_ES
dc.rights Reserva de todos los derechos es_ES
dc.subject Decomposition es_ES
dc.subject High resolution thermogravimetry es_ES
dc.subject Portland cement es_ES
dc.subject Variable heating rate es_ES
dc.subject Cement paste es_ES
dc.subject Cementitious materials es_ES
dc.subject Decomposition reaction es_ES
dc.subject High resolution es_ES
dc.subject High-resolution thermogravimetric analysis es_ES
dc.subject Mineral phasis es_ES
dc.subject Optimum parameters es_ES
dc.subject Portland cement paste es_ES
dc.subject Purge gas es_ES
dc.subject Reproducibilities es_ES
dc.subject Temperature range es_ES
dc.subject Heating rate es_ES
dc.subject Thermogravimetric analysis es_ES
dc.subject.classification High resolution thermogravimetry es_ES
dc.subject.classification Portland cement es_ES
dc.subject.classification Decomposition es_ES
dc.subject.classification Variable heating rate es_ES
dc.subject.classification INGENIERIA DE LA CONSTRUCCION es_ES
dc.title Determination of the optimum parameters in the high resolution thermogravimetric analysis (HRTG) for cementitious materials es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.1007/s10973-010-0997-0
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Departamento de Ingeniería de la Construcción y de Proyectos de Ingeniería Civil - Departament d'Enginyeria de la Construcció i de Projectes d'Enginyeria Civil es_ES
dc.description.bibliographicCitation Ivan Tobón, J.; Paya Bernabeu, JJ.; Borrachero Rosado, MV.; Soriano Martinez, L.; Restrepo Baena, OJ. (2012). Determination of the optimum parameters in the high resolution thermogravimetric analysis (HRTG) for cementitious materials. Journal of Thermal Analysis and Calorimetry. 107:233-239. doi:10.1007/s10973-010-0997-0 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion http://dx.doi.org/10.1007/s10973-010-0997-0 es_ES
dc.description.upvformatpinicio 233 es_ES
dc.description.upvformatpfin 239 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 107 es_ES
dc.relation.senia 212743
dc.identifier.eissn 1572-8943
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