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Preparation and Characterization of Electrospun Pectin-Based Films and Their Application in Sustainable Aroma Barrier Multilayer Packaging

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Preparation and Characterization of Electrospun Pectin-Based Films and Their Application in Sustainable Aroma Barrier Multilayer Packaging

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dc.contributor.author Balik, Busra Akinalan es_ES
dc.contributor.author Argin, Sanem es_ES
dc.contributor.author Lagaron, Jose M. es_ES
dc.contributor.author Torres-Giner, S. es_ES
dc.date.accessioned 2021-05-13T03:32:18Z
dc.date.available 2021-05-13T03:32:18Z
dc.date.issued 2019-11-27 es_ES
dc.identifier.uri http://hdl.handle.net/10251/166267
dc.description.abstract [EN] Featured Application: The present study aims to develop novel pectin-based films by electrospinning. The here -prepared films were applied as aroma barrier interlayers between two biopolymer films to develop fully bio-based and biodegradable food packaging articles according to the principles of the Circular Economy. Pectin was first dissolved in distilled water and blended with low contents of polyethylene oxide 2000 (PEO2000) as the carrier polymer to produce electrospun fibers. The electrospinning of the water solution of pectin at 9.5 wt% containing 0.5 wt% PEO2000 was selected as it successfully resulted in continuous and non-defected ultrathin fibers with the highest pectin content. However, annealing of the resultant pectin-based fibers, tested at different conditions, developed films with low mechanical integrity, high porosity, and also dark color due to their poor thermal stability. Then, to improve the film-forming process of the electrospun mats, two plasticizers, namely glycerol and polyethylene glycol 900 (PEG(900)), were added to the selected pectin solution in the 2-3 wt% range. The optimal annealing conditions were found at 150 degrees C with a pressure of 12 kN load for 1 min when applied to the electrospun pectin mats containing 5 wt% PEO2000 and 30 wt% glycerol and washed previously with dichloromethane. This process led to completely homogenous films with low porosity and high transparency due to a phenomenon of fibers coalescence. Finally, the selected electrospun pectin-based film was applied as an interlayer between two external layers of poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) by the electrospinning coating technology and the whole structure was annealed to produce a fully bio-based and biodegradable multilayer film with enhanced barrier performance to water vapor and limonene. es_ES
dc.description.sponsorship This study was supported by the Turkish Scientific and Technological Research Council (TUBITAK) 2214-A International Research Fellowship Programme for PhD Students and by the Spanish Ministry of Science, Innovation, and Universities (MICIU) project numbers AGL2015-63855-C2-1-R. S.T.-G. is a recipient of a Juan de la Cierva¿Incorporación contract (IJCI-2016-29675) from MICIU. es_ES
dc.language Inglés es_ES
dc.publisher MDPI AG es_ES
dc.relation.ispartof Applied Sciences es_ES
dc.rights Reconocimiento (by) es_ES
dc.subject Pectin es_ES
dc.subject Electrospinning es_ES
dc.subject Annealing es_ES
dc.subject Barrier interlayers es_ES
dc.subject Food packaging es_ES
dc.subject.classification CIENCIA DE LOS MATERIALES E INGENIERIA METALURGICA es_ES
dc.title Preparation and Characterization of Electrospun Pectin-Based Films and Their Application in Sustainable Aroma Barrier Multilayer Packaging es_ES
dc.type Artículo es_ES
dc.identifier.doi 10.3390/app9235136 es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//IJCI-2016-29675/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/MINECO//AGL2015-63855-C2-1-R/ES/DESARROLLO DE UN CONCEPTO DE ENVASE MULTICAPA ALIMENTARIO DE ALTA BARRERA Y CON CARACTER ACTIVO Y BIOACTIVO DERIVADO DE SUBPRODUCTOS ALIMENTARIOS/ es_ES
dc.relation.projectID info:eu-repo/grantAgreement/TUBITAK//2214-A/ es_ES
dc.rights.accessRights Abierto es_ES
dc.contributor.affiliation Universitat Politècnica de València. Instituto Universitario de Ingeniería de Alimentos para el Desarrollo - Institut Universitari d'Enginyeria d'Aliments per al Desenvolupament es_ES
dc.description.bibliographicCitation Balik, BA.; Argin, S.; Lagaron, JM.; Torres-Giner, S. (2019). Preparation and Characterization of Electrospun Pectin-Based Films and Their Application in Sustainable Aroma Barrier Multilayer Packaging. Applied Sciences. 9(23):1-24. https://doi.org/10.3390/app9235136 es_ES
dc.description.accrualMethod S es_ES
dc.relation.publisherversion https://doi.org/10.3390/app9235136 es_ES
dc.description.upvformatpinicio 1 es_ES
dc.description.upvformatpfin 24 es_ES
dc.type.version info:eu-repo/semantics/publishedVersion es_ES
dc.description.volume 9 es_ES
dc.description.issue 23 es_ES
dc.identifier.eissn 2076-3417 es_ES
dc.relation.pasarela S\427474 es_ES
dc.contributor.funder Technological Research Council of Turkey es_ES
dc.contributor.funder Ministerio de Economía y Competitividad es_ES
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dc.subject.ods 12.- Garantizar las pautas de consumo y de producción sostenibles es_ES


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